C₃₈H₆₅FO₂Si₂

Base Information

Chemical Name:C₃₈H₆₅FO₂Si₂
CAS No.:199798-99-7
Molecular Formula:C₃₈H₆₅FO₂Si₂
Molecular Weight:629.102
Hs Code.:

C<sub>38</sub>H<sub>65</sub>FO<sub>2</sub>Si<sub>2</sub>

Synonyms:C₃₈H₆₅FO₂Si₂

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Chemical Property of C₃₈H₆₅FO₂Si₂

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Technology Process of C₃₈H₆₅FO₂Si₂

There total 19 articles about C₃₈H₆₅FO₂Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 926315-11-9
(3aR,4S,7aR)-1-((S,E)-5-ethyl-5-hydroxy-1-methyl-hept-3-enyl)-7a-methyl-3a,4,5,6,7,7a-hexahydro-3H-inden-4-one

: 123836-63-5
<3S-(1Z,3α,5β)>-<2-<3-Fluoro-5-<<(1,1-dimethylethyl)dimethylsilyl>oxy>-2-methylenecyclohexylidene>ethyl>diphenylphosphine Oxide

: 199798-99-7
C₃₈H₆₅FO₂Si₂

Guidance literature:: <3S-(1Z,3α,5β)>-<2-<3-Fluoro-5-<<(1,1-dimethylethyl)dimethylsilyl>oxy>-2-methylenecyclohexylidene>ethyl>diphenylphosphine Oxide; With n-butyllithium; In tetrahydrofuran; hexane; at -75 ℃; for 0.333333h;

(3aR,4S,7aR)-1-((S,E)-5-ethyl-5-hydroxy-1-methyl-hept-3-enyl)-7a-methyl-3a,4,5,6,7,7a-hexahydro-3H-inden-4-one; In tetrahydrofuran; hexane; at -50 - -10 ℃; for 2.08333h; Product distribution / selectivity;

Reference yield:

: 926315-16-4
acetic acid (2R,3aR,4S,7aR,Z)-1-ethylidene-2-hydroxy-7a-methyl-octahydro-1H-inden-4-yl ester

: 199798-99-7
C₃₈H₆₅FO₂Si₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: mercury(II) diacetate / 18 h / 130 °C

2.1: lithium hexamethyldisilazane / tetrahydrofuran; hexane / 1.5 h / -100 - 78 °C

3.1: cerium(III) chloride / tetrahydrofuran; water / 26.33 h / 0 - 210 °C / 0.01 - 0.08 Torr

3.2: 0.67 - 2 h / 0 °C

4.1: dipyridinium dichromate / dichloromethane / 0 - 20 °C

5.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -75 °C

5.2: 2.08 h / -50 - -10 °C

With dipyridinium dichromate; n-butyllithium; cerium(III) chloride; mercury(II) diacetate; lithium hexamethyldisilazane; In tetrahydrofuran; hexane; dichloromethane; water;

Reference yield:

: 926315-12-0
benzoic acid (2R,3S,7S)-7-((t-butyldimethyl)silanyloxy)-4-methylene-1-oxa-spiro[2.5]oct-2-yl methyl ester

: 199798-99-7
C₃₈H₆₅FO₂Si₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: selenium(IV) oxide; di-tert-butyl peroxide / 1,4-dioxane; nonane / 22 - 37 h / 85 °C

2.1: diethylamino-sulfur trifluoride / Trichloroethylene / 0.33 h / -75 °C

3.1: triphenylphosphine / tris(3,5-dimethylpyrazolyl)hydriborate rhenium trioxide / toluene / 20 h / 100 °C

4.1: sodium methylate / methanol / 1 h / 20 °C

5.1: bis(trichloromethyl) carbonate / hexane / 0.5 h / 0 °C

5.2: 1 h / 0 - 20 °C

6.1: sodium hydride / N,N-dimethyl-formamide / 0.75 h / 10 - 20 °C

6.2: 3 h / -60 - 20 °C

7.1: lithium hexamethyldisilazane / tetrahydrofuran; toluene / 0.08 h / -55 °C

With selenium(IV) oxide; di-tert-butyl peroxide; bis(trichloromethyl) carbonate; diethylamino-sulfur trifluoride; sodium methylate; sodium hydride; triphenylphosphine; lithium hexamethyldisilazane; tris(3,5-dimethylpyrazolyl)hydriborate rhenium trioxide; In tetrahydrofuran; 1,4-dioxane; methanol; nonane; hexane; Trichloroethylene; N,N-dimethyl-formamide; toluene;