dibenzyl 2-((R)-2-formyl-1-(2-(3,4-dihydroisoquinolin-2(1H)-yl)phenyl)ethyl)malonate

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Chemical Name:dibenzyl 2-((R)-2-formyl-1-(2-(3,4-dihydroisoquinolin-2(1H)-yl)phenyl)ethyl)malonate
CAS No.:1407535-56-1
Molecular Formula:C₃₅H₃₃NO₅
Molecular Weight:547.651
Hs Code.:

Synonyms:dibenzyl 2-((R)-2-formyl-1-(2-(3,4-dihydroisoquinolin-2(1H)-yl)phenyl)ethyl)malonate

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Chemical Property of dibenzyl 2-((R)-2-formyl-1-(2-(3,4-dihydroisoquinolin-2(1H)-yl)phenyl)ethyl)malonate

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Technology Process of dibenzyl 2-((R)-2-formyl-1-(2-(3,4-dihydroisoquinolin-2(1H)-yl)phenyl)ethyl)malonate

There total 1 articles about dibenzyl 2-((R)-2-formyl-1-(2-(3,4-dihydroisoquinolin-2(1H)-yl)phenyl)ethyl)malonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 15014-25-2
malonic acid dibenzyl ester

: 1240591-76-7
C₁₈H₁₇NO

: 1407535-56-1
dibenzyl 2-((R)-2-formyl-1-(2-(3,4-dihydroisoquinolin-2(1H)-yl)phenyl)ethyl)malonate

Guidance literature:: With (2S)-2-{diphenyl[(trimethylsilyl)oxy]methyl}pyrrolidine; In tetrahydrofuran; at 20 ℃; enantioselective reaction;
DOI:10.1016/j.tetasy.2012.08.004

Reference yield: 25.0%

: 1407535-56-1
dibenzyl 2-((R)-2-formyl-1-(2-(3,4-dihydroisoquinolin-2(1H)-yl)phenyl)ethyl)malonate

: (13R)-dibenzyl 13-(formylmethyl)-6,7-dihydro-11bH-isoquinolino[2,1-a]quinoline-12,12(13H)-dicarboxylate

Guidance literature:: With sodium hydrogencarbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 0.5h;
DOI:10.1016/j.tetasy.2012.08.004