[2-(2-bromophenyl)-1-benzofuran-3-yl]methyl 2-(trimethylsilyl)ethyl ether

Base Information

Chemical Name:[2-(2-bromophenyl)-1-benzofuran-3-yl]methyl 2-(trimethylsilyl)ethyl ether
CAS No.:870010-88-1
Molecular Formula:C₂₀H₂₃BrO₂Si
Molecular Weight:403.391
Hs Code.:

Synonyms:[2-(2-bromophenyl)-1-benzofuran-3-yl]methyl 2-(trimethylsilyl)ethyl ether

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Chemical Property of [2-(2-bromophenyl)-1-benzofuran-3-yl]methyl 2-(trimethylsilyl)ethyl ether

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Technology Process of [2-(2-bromophenyl)-1-benzofuran-3-yl]methyl 2-(trimethylsilyl)ethyl ether

There total 4 articles about [2-(2-bromophenyl)-1-benzofuran-3-yl]methyl 2-(trimethylsilyl)ethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 870010-41-6
[2-({2-[(2-bromophenyl)ethynyl]phenoxy}methoxy)ethyl](trimethyl)silane

: 870010-88-1
[2-(2-bromophenyl)-1-benzofuran-3-yl]methyl 2-(trimethylsilyl)ethyl ether

Guidance literature:: With carbon monoxide; platinum(II) chloride; In toluene; at 80 ℃; for 3h; under 760 Torr;
DOI:10.1021/ja055659p

Reference yield:

: 870010-42-7
{2-[(2-iodophenoxy)methoxy]ethyl}(trimethyl)silane

: 870010-88-1
[2-(2-bromophenyl)-1-benzofuran-3-yl]methyl 2-(trimethylsilyl)ethyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: PdCl₂(PPh₃)2; CuI; Et₃N / 50 °C

2: 75 percent / PtCl₂; CO / toluene / 3 h / 80 °C / 760 Torr

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; carbon monoxide; triethylamine; platinum(II) chloride; In toluene; 1: Sonagashira reaction;
DOI:10.1021/ja055659p

Reference yield:

: 533-58-4
2-Iodophenol

: 870010-88-1
[2-(2-bromophenyl)-1-benzofuran-3-yl]methyl 2-(trimethylsilyl)ethyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / K₂CO₃ / acetonitrile / 20 °C

2: PdCl₂(PPh₃)2; CuI; Et₃N / 50 °C

3: 75 percent / PtCl₂; CO / toluene / 3 h / 80 °C / 760 Torr

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; carbon monoxide; potassium carbonate; triethylamine; platinum(II) chloride; In toluene; acetonitrile; 2: Sonagashira reaction;
DOI:10.1021/ja055659p