bis-(2,6-diisopropylphenyl)chlorophosphite

Base Information

• Chemical Name: bis-(2,6-diisopropylphenyl)chlorophosphite
• CAS No.: 174300-30-2
• Molecular Formula: C₂₄H₃₄ClO₂P
• Molecular Weight: 420.96

Synonyms:bis-(2,6-diisopropylphenyl)chlorophosphite

Chemical Property of bis-(2,6-diisopropylphenyl)chlorophosphite

Chemical Property:

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Technology Process of bis-(2,6-diisopropylphenyl)chlorophosphite

There total 1 articles about bis-(2,6-diisopropylphenyl)chlorophosphite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,6-diisopropylphenol (2078-54-8) → bis-(2,6-diisopropylphenyl)chlorophosphite (174300-30-2)

Guidance literature:

With phosphorus trichloride; In tetrahydrofuran; at 25 ℃; for 6h; Inert atmosphere;

DOI:10.1016/j.tet.2013.12.040

Reference yield: 86.0%

(2S,3S)-2-[(ferrocenylidene)-amino]-3-methyl-pentan-1-ol + bis-(2,6-diisopropylphenyl)chlorophosphite (174300-30-2) → (2S,3S)-bis-(2,6-diisopropylphenyl)-2-[(ferrocenylidene)-amino]-3-methyl-pentylphosphite

Guidance literature:

With triethylamine; In benzene; byproducts: Et3N*HCl; (Ar), chlorophosphite in benzene added dropwise to a stirred soln. of Fecomplex and Et3M in benzene at 0,degree.C, heated to boiling, cooled, s tirred at 50°C for 1 h; cooled to room temp., filtered, evapd.(vac.), dissolved (hexane), filtered, evapd.(vac.), elem. anal.;

DOI:10.1016/j.molcata.2006.06.025

upstream raw materials:

2,6-diisopropylphenol

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