methyl 3-(1-(tert-butyldimethylsilyloxy)-7-phenylheptyl)-1,2,4-oxadiazole-5-carboxylate

Base Information

• Chemical Name: methyl 3-(1-(tert-butyldimethylsilyloxy)-7-phenylheptyl)-1,2,4-oxadiazole-5-carboxylate
• CAS No.: 1042152-25-9
• Molecular Formula: C₂₃H₃₆N₂O₄Si
• Molecular Weight: 432.635

Synonyms:methyl 3-(1-(tert-butyldimethylsilyloxy)-7-phenylheptyl)-1,2,4-oxadiazole-5-carboxylate

Chemical Property of methyl 3-(1-(tert-butyldimethylsilyloxy)-7-phenylheptyl)-1,2,4-oxadiazole-5-carboxylate

Chemical Property:

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Technology Process of methyl 3-(1-(tert-butyldimethylsilyloxy)-7-phenylheptyl)-1,2,4-oxadiazole-5-carboxylate

There total 2 articles about methyl 3-(1-(tert-butyldimethylsilyloxy)-7-phenylheptyl)-1,2,4-oxadiazole-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

→ methyl 3-(1-(tert-butyldimethylsilyloxy)-7-phenylheptyl)-1,2,4-oxadiazole-5-carboxylate (1042152-25-9)

Guidance literature:

Reference yield:

monomethyl oxalyl chloride (5781-53-3) + C20H36N2O2Si (1042151-93-8) → methyl 3-(1-(tert-butyldimethylsilyloxy)-7-phenylheptyl)-1,2,4-oxadiazole-5-carboxylate (1042152-25-9)

Guidance literature:

monomethyl oxalyl chloride; C₂₀H₃₆N₂O₂Si; With triethylamine; In 1,2-dichloro-ethane; at 20 ℃; for 6h;

With p-toluenesulfonyl chloride; In 1,2-dichloro-ethane; at 80 ℃; for 16h; Inert atmosphere;

DOI:10.1021/jm800136b

Reference yield: 100.0%

methyl 3-(1-(tert-butyldimethylsilyloxy)-7-phenylheptyl)-1,2,4-oxadiazole-5-carboxylate (1042152-25-9) → methyl 3-(1-hydroxy-7-phenylheptyl)-1,2,4-oxadiazole-5-carboxylate (1042152-27-1)

Guidance literature:

With pyridine; pyridine hydrogenfluoride; In tetrahydrofuran; at 25 ℃; for 24h;

DOI:10.1021/jm800136b

upstream raw materials:

monomethyl oxalyl chloride

C₂₀H₃₆N₂O₂Si

Downstream raw materials:

methyl 3-(1-hydroxy-7-phenylheptyl)-1,2,4-oxadiazole-5-carboxylate

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