(1S)-2,3,4,6-tetra-O-acetyl-1,5-anhydro-D-glucitol-spiro[1.5]-3-(4-methoxyphenyl)-1,4,2-oxathiazole

Base Information

• Chemical Name: (1S)-2,3,4,6-tetra-O-acetyl-1,5-anhydro-D-glucitol-spiro[1.5]-3-(4-methoxyphenyl)-1,4,2-oxathiazole
• CAS No.: 1089209-16-4
• Molecular Formula: C₂₂H₂₅NO₁₁S
• Molecular Weight: 511.507

Synonyms:(1S)-2,3,4,6-tetra-O-acetyl-1,5-anhydro-D-glucitol-spiro[1.5]-3-(4-methoxyphenyl)-1,4,2-oxathiazole

Chemical Property of (1S)-2,3,4,6-tetra-O-acetyl-1,5-anhydro-D-glucitol-spiro[1.5]-3-(4-methoxyphenyl)-1,4,2-oxathiazole

Chemical Property:

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Technology Process of (1S)-2,3,4,6-tetra-O-acetyl-1,5-anhydro-D-glucitol-spiro[1.5]-3-(4-methoxyphenyl)-1,4,2-oxathiazole

There total 1 articles about (1S)-2,3,4,6-tetra-O-acetyl-1,5-anhydro-D-glucitol-spiro[1.5]-3-(4-methoxyphenyl)-1,4,2-oxathiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

C22H27NO11S (1089209-14-2) → (1S)-2,3,4,6-tetra-O-acetyl-1,5-anhydro-D-glucitol-spiro[1.5]-3-(4-methoxyphenyl)-1,4,2-oxathiazole (1089209-16-4)

Guidance literature:

With N-Bromosuccinimide; In tetrachloromethane; for 0.75h; Reflux; heat lamp illumination;

DOI:10.1016/j.bmcl.2008.08.052

Reference yield: 79.0%

(1S)-2,3,4,6-tetra-O-acetyl-1,5-anhydro-D-glucitol-spiro[1.5]-3-(4-methoxyphenyl)-1,4,2-oxathiazole (1089209-16-4) → (1S)-1,5-anhydro-D-glucitol-spiro[1.5]-3-(4-methoxyphenyl)-1,4,2-oxathiazole (1089209-19-7)

Guidance literature:

With methanol; sodium methylate; at 20 ℃; for 3h;

DOI:10.1016/j.bmcl.2008.08.052

upstream raw materials:

C₂₂H₂₇NO₁₁S

Downstream raw materials:

(1S)-1,5-anhydro-D-glucitol-spiro[1.5]-3-(4-methoxyphenyl)-1,4,2-oxathiazole

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