3-{2-amino-4-[4-(difluoromethoxy)phenyl]-1-methyl-5-oxo-4,5-dihydro-1H-imidazol-4-yl}benzaldehyde

Base Information

Chemical Name:3-{2-amino-4-[4-(difluoromethoxy)phenyl]-1-methyl-5-oxo-4,5-dihydro-1H-imidazol-4-yl}benzaldehyde
CAS No.:931429-87-7
Molecular Formula:C₁₈H₁₅F₂N₃O₃
Molecular Weight:359.332
Hs Code.:

Synonyms:3-{2-amino-4-[4-(difluoromethoxy)phenyl]-1-methyl-5-oxo-4,5-dihydro-1H-imidazol-4-yl}benzaldehyde

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Chemical Property of 3-{2-amino-4-[4-(difluoromethoxy)phenyl]-1-methyl-5-oxo-4,5-dihydro-1H-imidazol-4-yl}benzaldehyde

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Technology Process of 3-{2-amino-4-[4-(difluoromethoxy)phenyl]-1-methyl-5-oxo-4,5-dihydro-1H-imidazol-4-yl}benzaldehyde

There total 1 articles about 3-{2-amino-4-[4-(difluoromethoxy)phenyl]-1-methyl-5-oxo-4,5-dihydro-1H-imidazol-4-yl}benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 3-[2-(4-Difluoromethoxy-phenyl)-2-oxo-acetyl]-benzaldehyde

: 22661-87-6,21770-81-0
1-methylguanidine hydrochloride

: 931429-87-7
3-{2-amino-4-[4-(difluoromethoxy)phenyl]-1-methyl-5-oxo-4,5-dihydro-1H-imidazol-4-yl}benzaldehyde

Guidance literature:: With sodium carbonate; In isopropyl alcohol; at 86 ℃; for 15.5h;

Reference yield: 93.0%

: 931429-87-7
3-{2-amino-4-[4-(difluoromethoxy)phenyl]-1-methyl-5-oxo-4,5-dihydro-1H-imidazol-4-yl}benzaldehyde

: 75-31-0
isopropylamine

: 1065166-28-0
2-amino-5-[4-(difluoromethoxy)phenyl]-5-{3-[(isopropylamino)methyl]phenyl}-3-methyl-3,5-dihydro-4H-imidazol-4-one

Guidance literature:: 3-{2-amino-4-[4-(difluoromethoxy)phenyl]-1-methyl-5-oxo-4,5-dihydro-1H-imidazol-4-yl}benzaldehyde; isopropylamine; In methanol; for 2h;

With sodium tetrahydroborate; In methanol; for 0.333333h;

With sodium hydroxide; water; In methanol;

Reference yield: 83.0%

: 931429-87-7
3-{2-amino-4-[4-(difluoromethoxy)phenyl]-1-methyl-5-oxo-4,5-dihydro-1H-imidazol-4-yl}benzaldehyde

: 75-04-7,85404-22-4
ethylamine

: 1065166-34-8
2-amino-5-[4-(difluoromethoxy)phenyl]-5-{3-[(ethylamino)methyl]phenyl}-3-methyl-3,5-dihydro-4H-imidazol-4-one

Guidance literature:: 3-{2-amino-4-[4-(difluoromethoxy)phenyl]-1-methyl-5-oxo-4,5-dihydro-1H-imidazol-4-yl}benzaldehyde; ethylamine; In tetrahydrofuran;

With sodium tetrahydroborate; In tetrahydrofuran; methanol; for 1h;

With sodium hydroxide; water; In tetrahydrofuran; methanol;