DL-2,2'-[6-(4-sulfamoylphenethylamino)-1,3,5-triazine-2,4-diyl]bis(azanediyl)bis(3-hydroxypropanoic acid)

Base Information

Chemical Name:DL-2,2'-[6-(4-sulfamoylphenethylamino)-1,3,5-triazine-2,4-diyl]bis(azanediyl)bis(3-hydroxypropanoic acid)
CAS No.:1311200-34-6
Molecular Formula:C₁₇H₂₃N₇O₈S
Molecular Weight:485.478
Hs Code.:

Synonyms:DL-2,2'-[6-(4-sulfamoylphenethylamino)-1,3,5-triazine-2,4-diyl]bis(azanediyl)bis(3-hydroxypropanoic acid)

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Chemical Property of DL-2,2'-[6-(4-sulfamoylphenethylamino)-1,3,5-triazine-2,4-diyl]bis(azanediyl)bis(3-hydroxypropanoic acid)

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Technology Process of DL-2,2'-[6-(4-sulfamoylphenethylamino)-1,3,5-triazine-2,4-diyl]bis(azanediyl)bis(3-hydroxypropanoic acid)

There total 2 articles about DL-2,2'-[6-(4-sulfamoylphenethylamino)-1,3,5-triazine-2,4-diyl]bis(azanediyl)bis(3-hydroxypropanoic acid) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 302-84-1,83245-15-2
serin

: 796871-27-7
4-{2-[(4,6-dichloro-1,3,5-triazin-2-yl)amino]ethyl}benzene-1-sulfonamide

: 1311200-34-6
DL-2,2'-[6-(4-sulfamoylphenethylamino)-1,3,5-triazine-2,4-diyl]bis(azanediyl)bis(3-hydroxypropanoic acid)

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.bmc.2011.04.005

Reference yield:

: 35303-76-5
4-(2-aminoethyl)benzenesulfonamide

: 1311200-34-6
DL-2,2'-[6-(4-sulfamoylphenethylamino)-1,3,5-triazine-2,4-diyl]bis(azanediyl)bis(3-hydroxypropanoic acid)

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetone / 0 °C

1.2: 1.33 h

2.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.bmc.2011.04.005