Acetic acid (1S,2S,5R,6S)-2,6-diacetoxy-3-acetoxymethyl-5-hydroxy-cyclohex-3-enyl ester

Base Information

Chemical Name:Acetic acid (1S,2S,5R,6S)-2,6-diacetoxy-3-acetoxymethyl-5-hydroxy-cyclohex-3-enyl ester
CAS No.:775348-83-9
Molecular Formula:C₁₅H₂₀O₉
Molecular Weight:344.318
Hs Code.:

Synonyms:Acetic acid (1S,2S,5R,6S)-2,6-diacetoxy-3-acetoxymethyl-5-hydroxy-cyclohex-3-enyl ester

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Chemical Property of Acetic acid (1S,2S,5R,6S)-2,6-diacetoxy-3-acetoxymethyl-5-hydroxy-cyclohex-3-enyl ester

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Technology Process of Acetic acid (1S,2S,5R,6S)-2,6-diacetoxy-3-acetoxymethyl-5-hydroxy-cyclohex-3-enyl ester

There total 1 articles about Acetic acid (1S,2S,5R,6S)-2,6-diacetoxy-3-acetoxymethyl-5-hydroxy-cyclohex-3-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 774599-21-2
Acetic acid (1S,2S,6R)-2,6-diacetoxy-3-acetoxymethyl-5-oxo-cyclohex-3-enyl ester

: 775348-83-9
Acetic acid (1S,2S,5R,6S)-2,6-diacetoxy-3-acetoxymethyl-5-hydroxy-cyclohex-3-enyl ester

Guidance literature:: With sodium tetrahydroborate; cerium(III) chloride; In methanol; at -7 ℃; for 1.5h;
DOI:10.1021/ol0490779

Reference yield: 84.0%

: 775348-83-9
Acetic acid (1S,2S,5R,6S)-2,6-diacetoxy-3-acetoxymethyl-5-hydroxy-cyclohex-3-enyl ester

: 774599-42-7
N-tert-butoxycarbonyl-glycine-L-cysteine-L-phenylalanine ethyl ester

: 774599-30-3
(S)-2-[(R)-2-(2-tert-Butoxycarbonylamino-acetylamino)-3-((1S,4S,5S,6R)-4,5,6-triacetoxy-3-acetoxymethyl-cyclohex-2-enylsulfanyl)-propionylamino]-3-phenyl-propionic acid ethyl ester

Guidance literature:: Acetic acid (1S,2S,5R,6S)-2,6-diacetoxy-3-acetoxymethyl-5-hydroxy-cyclohex-3-enyl ester; With pyridine; methanesulfonyl chloride; In dichloromethane; at 20 ℃; for 1h;

N-tert-butoxycarbonyl-glycine-L-cysteine-L-phenylalanine ethyl ester; In water; N,N-dimethyl-formamide; at 20 ℃; for 6h;
DOI:10.1021/ol0490779

Reference yield: 76.0%

: 775348-83-9
Acetic acid (1S,2S,5R,6S)-2,6-diacetoxy-3-acetoxymethyl-5-hydroxy-cyclohex-3-enyl ester

: 172749-96-1
N-[(tert-butoxy)carbonyl]-L-cysteine methyl ester

: 774599-29-0
(R)-2-tert-Butoxycarbonylamino-3-((1S,4S,5S,6R)-4,5,6-triacetoxy-3-acetoxymethyl-cyclohex-2-enylsulfanyl)-propionic acid methyl ester

Guidance literature:: Acetic acid (1S,2S,5R,6S)-2,6-diacetoxy-3-acetoxymethyl-5-hydroxy-cyclohex-3-enyl ester; With pyridine; methanesulfonyl chloride; In dichloromethane; at 20 ℃; for 1h;

N-[(tert-butoxy)carbonyl]-L-cysteine methyl ester; In water; N,N-dimethyl-formamide; at 20 ℃; for 2.5h;
DOI:10.1021/ol0490779