7α-<(1R)-1-hydroxy-1-methyl-3-<4-(allyloxy)phenyl>propyl>-6,14-endo-ethenotetrahydro-N-(cyclopropylmethyl)northebaine

Base Information

Chemical Name:7α-<(1R)-1-hydroxy-1-methyl-3-<4-(allyloxy)phenyl>propyl>-6,14-endo-ethenotetrahydro-N-(cyclopropylmethyl)northebaine
CAS No.:98704-53-1
Molecular Formula:C₃₇H₄₅NO₅
Molecular Weight:583.768
Hs Code.:

Synonyms:7α-<(1R)-1-hydroxy-1-methyl-3-<4-(allyloxy)phenyl>propyl>-6,14-endo-ethenotetrahydro-N-(cyclopropylmethyl)northebaine

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Chemical Property of 7α-<(1R)-1-hydroxy-1-methyl-3-<4-(allyloxy)phenyl>propyl>-6,14-endo-ethenotetrahydro-N-(cyclopropylmethyl)northebaine

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Technology Process of 7α-<(1R)-1-hydroxy-1-methyl-3-<4-(allyloxy)phenyl>propyl>-6,14-endo-ethenotetrahydro-N-(cyclopropylmethyl)northebaine

There total 5 articles about 7α-<(1R)-1-hydroxy-1-methyl-3-<4-(allyloxy)phenyl>propyl>-6,14-endo-ethenotetrahydro-N-(cyclopropylmethyl)northebaine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 7051-34-5
cyclopropylcarbinyl bromide

: 98704-52-0
7α-<(1R)-1-hydroxy-1-methyl-3-<4-(allyloxy)phenyl>propyl>-6,14-endo-ethenotetrahydronorthebaine

: 98704-53-1
7α-<(1R)-1-hydroxy-1-methyl-3-<4-(allyloxy)phenyl>propyl>-6,14-endo-ethenotetrahydro-N-(cyclopropylmethyl)northebaine

Guidance literature:: With sodium carbonate; sodium iodide; In water; acetone; for 3h; Heating;
DOI:10.1021/jm00150a032

Reference yield:

: C₁₁H₁₃BrMgO

: 98704-53-1
7α-<(1R)-1-hydroxy-1-methyl-3-<4-(allyloxy)phenyl>propyl>-6,14-endo-ethenotetrahydro-N-(cyclopropylmethyl)northebaine

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / 6 h / Heating

2: 1.) ethyl azodicarboxylate, 2.) NH₄Cl / 1.) benzene, reflux, 5 h, 2.) water, ethanol, heting, 7 h

3: 77 percent / NaI, Na₂CO₃ / acetone; H₂O / 3 h / Heating

With ethyl azodicarboxylate; sodium carbonate; ammonium chloride; sodium iodide; In tetrahydrofuran; water; acetone;
DOI:10.1021/jm00150a032

Reference yield:

: C₁₁H₁₃IMgO

: 98704-53-1
7α-<(1R)-1-hydroxy-1-methyl-3-<4-(allyloxy)phenyl>propyl>-6,14-endo-ethenotetrahydro-N-(cyclopropylmethyl)northebaine

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether / 24 h / Heating

2: 1.) ethyl azodicarboxylate, 2.) NH₄Cl / 1.) benzene, reflux, 5 h, 2.) water, ethanol, heting, 7 h

3: 77 percent / NaI, Na₂CO₃ / acetone; H₂O / 3 h / Heating

With ethyl azodicarboxylate; sodium carbonate; ammonium chloride; sodium iodide; In diethyl ether; water; acetone;
DOI:10.1021/jm00150a032