{6-[(1S,6R)-2-Benzenesulfonyl-6-(tert-butyl-dimethyl-silanyloxy)-2-(2-trimethylsilanyl-ethylsulfanyl)-cyclohexyl]-benzo[1,3]dioxol-5-yl}-methanol

Base Information

Chemical Name:{6-[(1S,6R)-2-Benzenesulfonyl-6-(tert-butyl-dimethyl-silanyloxy)-2-(2-trimethylsilanyl-ethylsulfanyl)-cyclohexyl]-benzo[1,3]dioxol-5-yl}-methanol
CAS No.:118419-51-5
Molecular Formula:C₃₁H₄₈O₆S₂Si₂
Molecular Weight:637.022
Hs Code.:

{6-[(1S,6R)-2-Benzenesulfonyl-6-(tert-butyl-dimethyl-silanyloxy)-2-(2-trimethylsilanyl-ethylsulfanyl)-cyclohexyl]-benzo[1,3]dioxol-5-yl}-methanol

Synonyms:{6-[(1S,6R)-2-Benzenesulfonyl-6-(tert-butyl-dimethyl-silanyloxy)-2-(2-trimethylsilanyl-ethylsulfanyl)-cyclohexyl]-benzo[1,3]dioxol-5-yl}-methanol

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Chemical Property of {6-[(1S,6R)-2-Benzenesulfonyl-6-(tert-butyl-dimethyl-silanyloxy)-2-(2-trimethylsilanyl-ethylsulfanyl)-cyclohexyl]-benzo[1,3]dioxol-5-yl}-methanol

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Technology Process of {6-[(1S,6R)-2-Benzenesulfonyl-6-(tert-butyl-dimethyl-silanyloxy)-2-(2-trimethylsilanyl-ethylsulfanyl)-cyclohexyl]-benzo[1,3]dioxol-5-yl}-methanol

There total 4 articles about {6-[(1S,6R)-2-Benzenesulfonyl-6-(tert-butyl-dimethyl-silanyloxy)-2-(2-trimethylsilanyl-ethylsulfanyl)-cyclohexyl]-benzo[1,3]dioxol-5-yl}-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 118419-50-4
6-[(1S,6R)-2-Benzenesulfonyl-6-(tert-butyl-dimethyl-silanyloxy)-2-(2-trimethylsilanyl-ethylsulfanyl)-cyclohexyl]-benzo[1,3]dioxole-5-carbaldehyde

: 118419-51-5
{6-[(1S,6R)-2-Benzenesulfonyl-6-(tert-butyl-dimethyl-silanyloxy)-2-(2-trimethylsilanyl-ethylsulfanyl)-cyclohexyl]-benzo[1,3]dioxol-5-yl}-methanol

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; methanol; for 0.166667h; Ambient temperature;
DOI:10.1021/ja00184a082

Reference yield:

: 118419-48-0
C₁₀H₉LiO₄

: 118419-51-5
{6-[(1S,6R)-2-Benzenesulfonyl-6-(tert-butyl-dimethyl-silanyloxy)-2-(2-trimethylsilanyl-ethylsulfanyl)-cyclohexyl]-benzo[1,3]dioxol-5-yl}-methanol

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) THF, ether, -78 deg C, 2.) 0 deg C

2: 93 percent / NaBH₄ / tetrahydrofuran; methanol / 0.17 h / Ambient temperature

With sodium tetrahydroborate; In tetrahydrofuran; methanol;
DOI:10.1021/ja00184a082

Reference yield:

: 118419-49-1
5-[(1S,6R)-2-Benzenesulfonyl-6-(tert-butyl-dimethyl-silanyloxy)-2-(2-trimethylsilanyl-ethylsulfanyl)-cyclohexyl]-6-[1,3]dioxolan-2-yl-benzo[1,3]dioxole

: 118419-51-5
{6-[(1S,6R)-2-Benzenesulfonyl-6-(tert-butyl-dimethyl-silanyloxy)-2-(2-trimethylsilanyl-ethylsulfanyl)-cyclohexyl]-benzo[1,3]dioxol-5-yl}-methanol

Guidance literature:: Multi-step reaction with 2 steps

1: p-toluenesulfonic acid / acetone / 2 h / 25 °C

2: 93 percent / NaBH₄ / tetrahydrofuran; methanol / 0.17 h / Ambient temperature

With sodium tetrahydroborate; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; acetone;
DOI:10.1021/ja00184a082