N-allyl-N-prop-2-ynyl-C-(4-vinyl-phenyl)-methanesulfonamide

Base Information

• Chemical Name: N-allyl-N-prop-2-ynyl-C-(4-vinyl-phenyl)-methanesulfonamide
• CAS No.: 423170-39-2
• Molecular Formula: C₁₅H₁₇NO₂S
• Molecular Weight: 275.371
• Mol file: 423170-39-2.mol

Synonyms:N-allyl-N-prop-2-ynyl-C-(4-vinyl-phenyl)-methanesulfonamide

Chemical Property of N-allyl-N-prop-2-ynyl-C-(4-vinyl-phenyl)-methanesulfonamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-allyl-N-prop-2-ynyl-C-(4-vinyl-phenyl)-methanesulfonamide

There total 2 articles about N-allyl-N-prop-2-ynyl-C-(4-vinyl-phenyl)-methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

propargyl bromide (106-96-7) + N-allyl-C-(4-vinyl-phenyl)-methanesulfonamide → N-allyl-N-prop-2-ynyl-C-(4-vinyl-phenyl)-methanesulfonamide (423170-39-2)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; toluene; at 20 ℃; for 15h;

DOI:10.1055/s-2002-19762

Reference yield:

(4-vinyl-phenyl)-methanesulfonyl chloride → N-allyl-N-prop-2-ynyl-C-(4-vinyl-phenyl)-methanesulfonamide (423170-39-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 79 percent / Et₃N / CH₂Cl₂ / 15 h / 20 °C

2: 92 percent / Cs₂CO₃ / dimethylformamide; toluene / 15 h / 20 °C

With caesium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide; toluene;

DOI:10.1055/s-2002-19762

upstream raw materials:

propargyl bromide