2,5-bis[m-[N-(1'S)-(1'-isopropyl-2'-chloroethyl)amido]phenyl]-1,3,4-oxadiazole

Base Information

Chemical Name:2,5-bis[m-[N-(1'S)-(1'-isopropyl-2'-chloroethyl)amido]phenyl]-1,3,4-oxadiazole
CAS No.:630106-26-2
Molecular Formula:C₂₆H₃₀Cl₂N₄O₃
Molecular Weight:517.455
Hs Code.:

Synonyms:2,5-bis[m-[N-(1'S)-(1'-isopropyl-2'-chloroethyl)amido]phenyl]-1,3,4-oxadiazole

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Chemical Property of 2,5-bis[m-[N-(1'S)-(1'-isopropyl-2'-chloroethyl)amido]phenyl]-1,3,4-oxadiazole

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Technology Process of 2,5-bis[m-[N-(1'S)-(1'-isopropyl-2'-chloroethyl)amido]phenyl]-1,3,4-oxadiazole

There total 3 articles about 2,5-bis[m-[N-(1'S)-(1'-isopropyl-2'-chloroethyl)amido]phenyl]-1,3,4-oxadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 630106-22-8
2,5-bis[m-[N-(1'S)-(1'-isopropyl-2'-hydroxyethyl)amido]phenyl]-1,3,4-oxadiazole

: 630106-26-2
2,5-bis[m-[N-(1'S)-(1'-isopropyl-2'-chloroethyl)amido]phenyl]-1,3,4-oxadiazole

Guidance literature:: With thionyl chloride; In dichloromethane; for 5h; Heating;
DOI:10.1081/SCC-120021848

Reference yield:

: 4416-76-6
3,3'-[1,3,4]oxadiazole-2,5-diyl-bis-benzoyl chloride

: 630106-26-2
2,5-bis[m-[N-(1'S)-(1'-isopropyl-2'-chloroethyl)amido]phenyl]-1,3,4-oxadiazole

Guidance literature:: Multi-step reaction with 2 steps

1: 1.9 g / Et₃N / CH₂Cl₂ / 24 h / 20 °C

2: 76 percent / SOCl₂ / CH₂Cl₂ / 5 h / Heating

With thionyl chloride; triethylamine; In dichloromethane;
DOI:10.1081/SCC-120021848

Reference yield:

: 2425-93-6
3,3'-(1,3,4-oxadiazole-2,5-diyl)dibenzoic acid

: 630106-26-2
2,5-bis[m-[N-(1'S)-(1'-isopropyl-2'-chloroethyl)amido]phenyl]-1,3,4-oxadiazole

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂ / 10 h / Heating

2: 1.9 g / Et₃N / CH₂Cl₂ / 24 h / 20 °C

3: 76 percent / SOCl₂ / CH₂Cl₂ / 5 h / Heating

With thionyl chloride; triethylamine; In dichloromethane;
DOI:10.1081/SCC-120021848