4(R)-<1-buten-3(R)-yl>-3(S)-<1(R)-<(tert-butyldiphenylsilyl)oxy>ethyl>-2-oxoazetidine

Base Information

Chemical Name:4(R)-<1-buten-3(R)-yl>-3(S)-<1(R)-<(tert-butyldiphenylsilyl)oxy>ethyl>-2-oxoazetidine
CAS No.:97466-00-7
Molecular Formula:C₂₅H₃₃NO₂Si
Molecular Weight:407.628
Hs Code.:

Synonyms:4(R)-<1-buten-3(R)-yl>-3(S)-<1(R)-<(tert-butyldiphenylsilyl)oxy>ethyl>-2-oxoazetidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4(R)-<1-buten-3(R)-yl>-3(S)-<1(R)-<(tert-butyldiphenylsilyl)oxy>ethyl>-2-oxoazetidine

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Technology Process of 4(R)-<1-buten-3(R)-yl>-3(S)-<1(R)-<(tert-butyldiphenylsilyl)oxy>ethyl>-2-oxoazetidine

There total 4 articles about 4(R)-<1-buten-3(R)-yl>-3(S)-<1(R)-<(tert-butyldiphenylsilyl)oxy>ethyl>-2-oxoazetidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 97415-93-5
3(S)-<1(R)-<(tert-butyldiphenylsilyl)oxy>ethyl>-4(R)-<(ethoxythiocarbonyl)thio>-2-oxoazetidine

: 97403-56-0
3(R)-<1(R)-<(tert-butyldiphenylsilyl)oxy>ethyl>-4(R)-ethoxy-2-oxoazetidine

: 97466-00-7
4(R)-<1-buten-3(R)-yl>-3(S)-<1(R)-<(tert-butyldiphenylsilyl)oxy>ethyl>-2-oxoazetidine

: 97403-58-2
4(R)-<1-buten-3(S)-yl>-3(S)-<1(R)-<(tert-butyldiphenylsilyl)oxy>ethyl>-2-oxoazetidine

Guidance literature:: With 2,2'-azobis(isobutyronitrile); crotyltributylstannane; In toluene; at 90 ℃; Yields of byproduct given;
DOI:10.1021/jo00219a003

Reference yield:

: 31197-41-8,76505-19-6
crotyltributylstannane

: 97403-52-6
4(R)-acetoxy-3(R)-<1(R)-<(tert-butyldiphenylsilyl)oxy>ethyl>-2-oxoazetidine

: 97466-00-7
4(R)-<1-buten-3(R)-yl>-3(S)-<1(R)-<(tert-butyldiphenylsilyl)oxy>ethyl>-2-oxoazetidine

: 97403-58-2
4(R)-<1-buten-3(S)-yl>-3(S)-<1(R)-<(tert-butyldiphenylsilyl)oxy>ethyl>-2-oxoazetidine

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; for 20h; Yield given. Yields of byproduct given; Ambient temperature;
DOI:10.1021/jo00219a003

Reference yield:

: 31197-41-8,76505-19-6
crotyltributylstannane

: 97403-54-8,97466-02-9
3-<1-<(tert-butyldiphenylsilyl)oxy>ethyl>-4-(ethylthio)-2-oxoazetidine S-oxide

: 97466-00-7
4(R)-<1-buten-3(R)-yl>-3(S)-<1(R)-<(tert-butyldiphenylsilyl)oxy>ethyl>-2-oxoazetidine

: 97403-58-2
4(R)-<1-buten-3(S)-yl>-3(S)-<1(R)-<(tert-butyldiphenylsilyl)oxy>ethyl>-2-oxoazetidine

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; for 20h; Yield given. Yields of byproduct given; Ambient temperature;
DOI:10.1021/jo00219a003