1H-Pyrrole-2,3-dimethanol,2,5-dihydro-1-methyl-

Base Information

Chemical Name:1H-Pyrrole-2,3-dimethanol,2,5-dihydro-1-methyl-
CAS No.:103252-60-4
Molecular Formula:C₇H₁₃NO₂
Molecular Weight:143.186
Hs Code.:
Mol file:103252-60-4.mol

Synonyms:2,3-Bis(hydroxymethyl)-1-methyl-3-pyrroline;Synthanecine A;1H-Pyrrole-2,3-dimethanol,2,5-dihydro-1-methyl-, (?à)-;2,3-Bis(hydroxymethyl)-1-methyl-3-pyrroline;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1H-Pyrrole-2,3-dimethanol,2,5-dihydro-1-methyl-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1H-Pyrrole-2,3-dimethanol,2,5-dihydro-1-methyl-

There total 4 articles about 1H-Pyrrole-2,3-dimethanol,2,5-dihydro-1-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-(Ethoxycarbonylmethyl-methyl-amino)-succinic acid 1-ethyl ester 4-propyl ester

: 103252-60-4,53365-59-6
(+/-)-synthanecine A

Guidance literature:: Multi-step reaction with 3 steps

1: NaH / toluene

2: 1) NaBH₄, 2percent NaOH; 2) 4-MeC₆H₄SO₂Cl / 2) pyridine

3: i-Bu₂AlH

With sodium hydroxide; sodium tetrahydroborate; sodium hydride; diisobutylaluminium hydride; p-toluenesulfonyl chloride; In toluene;

Reference yield:

: 53365-54-1
1-methyl-2,5-dihydro-pyrrole-2,3-dicarboxylic acid diethyl ester

: 103252-60-4,53365-59-6
(+/-)-synthanecine A

Guidance literature:: With diisobutylaluminium hydride;

Reference yield:

: 53365-50-7
1-methyl-4-oxo-pyrrolidine-2,3-dicarboxylic acid diethyl ester

: 103252-60-4,53365-59-6
(+/-)-synthanecine A

Guidance literature:: Multi-step reaction with 2 steps

1: 1) NaBH₄, 2percent NaOH; 2) 4-MeC₆H₄SO₂Cl / 2) pyridine

2: i-Bu₂AlH

With sodium hydroxide; sodium tetrahydroborate; diisobutylaluminium hydride; p-toluenesulfonyl chloride;