N-<(2R)-2-(1-naphthylmethyl)-3-(N-phenethylcarbamoyl)propionyl>-L-histidine methyl ester

Base Information

Chemical Name:N-<(2R)-2-(1-naphthylmethyl)-3-(N-phenethylcarbamoyl)propionyl>-L-histidine methyl ester
CAS No.:132488-68-7
Molecular Formula:C₃₀H₃₂N₄O₄
Molecular Weight:512.608
Hs Code.:

Synonyms:N-<(2R)-2-(1-naphthylmethyl)-3-(N-phenethylcarbamoyl)propionyl>-L-histidine methyl ester

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Chemical Property of N-<(2R)-2-(1-naphthylmethyl)-3-(N-phenethylcarbamoyl)propionyl>-L-histidine methyl ester

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Technology Process of N-<(2R)-2-(1-naphthylmethyl)-3-(N-phenethylcarbamoyl)propionyl>-L-histidine methyl ester

There total 1 articles about N-<(2R)-2-(1-naphthylmethyl)-3-(N-phenethylcarbamoyl)propionyl>-L-histidine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 120052-26-8
(R)-2-(1-Naphthylmethyl)-3-(N-phenethylcarbamoyl)propionic Acid

: 4467-54-3,5619-10-3,7389-87-9,18684-16-7,22888-60-4,32381-17-2,92742-29-5,100009-20-9
l-histidine methyl ester dihydrochloride

: 132488-68-7
N-<(2R)-2-(1-naphthylmethyl)-3-(N-phenethylcarbamoyl)propionyl>-L-histidine methyl ester

Guidance literature:: With diphenylphosphoranyl azide; triethylamine; In N,N-dimethyl-formamide; at 0 ℃; for 16h;
DOI:10.1248/cpb.38.3042

Reference yield: 93.0%

: 132488-68-7
N-<(2R)-2-(1-naphthylmethyl)-3-(N-phenethylcarbamoyl)propionyl>-L-histidine methyl ester

: 105227-75-6
N-<(2R)-2-(1-Naphthylmethyl)-3-(N-phenethylcarbamoyl)propionyl>-L-histidine Hydrazide

Guidance literature:: With hydrazine hydrate; In methanol; overnight;
DOI:10.1248/cpb.38.3042

Reference yield:

: 132488-68-7
N-<(2R)-2-(1-naphthylmethyl)-3-(N-phenethylcarbamoyl)propionyl>-L-histidine methyl ester

: (S)-3-(1H-Imidazol-4-yl)-2-[(R)-3-naphthalen-1-yl-2-(phenethylcarbamoyl-methyl)-propionylamino]-propionyl azide

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / hydrazine hydrate / methanol / overnight

2: isoamyl nitrite

With hydrazine hydrate; isopentyl nitrite; In methanol;
DOI:10.1248/cpb.38.3042