(3S)-8-benzoyloxylinaloyl 2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-β-D-glucopyranoside

Base Information

Chemical Name:(3S)-8-benzoyloxylinaloyl 2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-β-D-glucopyranoside
CAS No.:179090-79-0
Molecular Formula:C₇₀H₆₄O₁₈
Molecular Weight:1193.27
Hs Code.:

Synonyms:(3S)-8-benzoyloxylinaloyl 2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S)-8-benzoyloxylinaloyl 2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-β-D-glucopyranoside

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Technology Process of (3S)-8-benzoyloxylinaloyl 2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-β-D-glucopyranoside

There total 10 articles about (3S)-8-benzoyloxylinaloyl 2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 179090-77-8
(3S)-8-benzoyloxylinaloyl 2,3,4-tri-O-benzoyl-β-D-glucopyranoside

: 14262-83-0
2,3,4-tri-O-benzoyl-α-D-xylopyranosyl bromide

: 179090-79-0
(3S)-8-benzoyloxylinaloyl 2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-β-D-glucopyranoside

Guidance literature:: With 2,4,6-trimethyl-pyridine; silver trifluoromethanesulfonate; In dichloromethane;
DOI:10.1016/0040-4039(96)00750-2

Reference yield: 78.7%

: 179090-77-8
(3S)-8-benzoyloxylinaloyl 2,3,4-tri-O-benzoyl-β-D-glucopyranoside

: 14262-83-0
2,3,4-tri-O-benzoyl-α-D-xylopyranosyl bromide

: 179090-79-0
(3S)-8-benzoyloxylinaloyl 2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-β-D-glucopyranoside

: C₇₀H₆₄O₁₈

Guidance literature:: With 2,4,6-trimethyl-pyridine; 4 A molecular sieve; silver trifluoromethanesulfonate; In dichloromethane; toluene; at -20 ℃; for 15h;
DOI:10.1016/S0008-6215(97)00086-4

Reference yield:

: 193695-39-5
8-benzoyloxylinaloyl 2,3,4-tri-O-benzoyl-6-O-chloroacetyl-β-D-glucopyranoside

: 179090-79-0
(3S)-8-benzoyloxylinaloyl 2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; triethylamine; Cysteamine / methanol

2: 2,4,6-trimethyl-pyridine; silver trifluoromethanesulfonate / dichloromethane

With pyridine; 2,4,6-trimethyl-pyridine; silver trifluoromethanesulfonate; triethylamine; Cysteamine; In methanol; dichloromethane;
DOI:10.1016/0040-4039(96)00750-2