methyl 2-[N-acetyl-N-(tert-butoxycarbonyl)amino]-3,4,6-tri-O-(4-tert-butylbenzyl)-2-deoxy-α-D-glucopyranoside

Base Information

Chemical Name:methyl 2-[N-acetyl-N-(tert-butoxycarbonyl)amino]-3,4,6-tri-O-(4-tert-butylbenzyl)-2-deoxy-α-D-glucopyranoside
CAS No.:1281971-20-7
Molecular Formula:C₄₇H₆₇NO₈
Molecular Weight:774.051
Hs Code.:

Synonyms:methyl 2-[N-acetyl-N-(tert-butoxycarbonyl)amino]-3,4,6-tri-O-(4-tert-butylbenzyl)-2-deoxy-α-D-glucopyranoside

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Chemical Property of methyl 2-[N-acetyl-N-(tert-butoxycarbonyl)amino]-3,4,6-tri-O-(4-tert-butylbenzyl)-2-deoxy-α-D-glucopyranoside

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Technology Process of methyl 2-[N-acetyl-N-(tert-butoxycarbonyl)amino]-3,4,6-tri-O-(4-tert-butylbenzyl)-2-deoxy-α-D-glucopyranoside

There total 4 articles about methyl 2-[N-acetyl-N-(tert-butoxycarbonyl)amino]-3,4,6-tri-O-(4-tert-butylbenzyl)-2-deoxy-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1281971-18-3
methyl 2-(N-acetylamino)-3,4,6-tri-O-(4-tert-butylbenzyl)-2-deoxy-α-D-glucopyranoside

: 1281971-20-7
methyl 2-[N-acetyl-N-(tert-butoxycarbonyl)amino]-3,4,6-tri-O-(4-tert-butylbenzyl)-2-deoxy-α-D-glucopyranoside

Guidance literature:: With dmap; In tetrahydrofuran; for 8h; Reflux;
DOI:10.1021/jo1023156

Reference yield:

: 3055-46-7,3946-01-8,5627-24-7,6082-04-8,6082-22-0,17327-09-2,22256-76-4,32087-35-7,32087-36-8,95341-97-2,114029-61-7,114612-10-1,114612-13-4,116559-74-1
methyl N-acetyl-D-glucosamine

: 1281971-20-7
methyl 2-[N-acetyl-N-(tert-butoxycarbonyl)amino]-3,4,6-tri-O-(4-tert-butylbenzyl)-2-deoxy-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C

2: dmap / tetrahydrofuran / 8 h / Reflux

With dmap; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/jo1023156

Reference yield:

: 18880-00-7
1-(bromomethyl)-4-(1,1-dimethylethyl)benzene

: 1281971-20-7
methyl 2-[N-acetyl-N-(tert-butoxycarbonyl)amino]-3,4,6-tri-O-(4-tert-butylbenzyl)-2-deoxy-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 3 h / 0 - 20 °C

2: dmap / tetrahydrofuran / 42 h / Reflux

With dmap; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;
DOI:10.1002/ejoc.201200522