diphenyl 1-amino-2-{4-[N,N'-bis(tert-butyloxycarbonyl)guanidino]phenyl}ethanephosphonate

Base Information

Chemical Name:diphenyl 1-amino-2-{4-[N,N'-bis(tert-butyloxycarbonyl)guanidino]phenyl}ethanephosphonate
CAS No.:913239-29-9
Molecular Formula:C₃₁H₃₉N₄O₇P
Molecular Weight:610.647
Hs Code.:

Synonyms:diphenyl 1-amino-2-{4-[N,N'-bis(tert-butyloxycarbonyl)guanidino]phenyl}ethanephosphonate

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Chemical Property of diphenyl 1-amino-2-{4-[N,N'-bis(tert-butyloxycarbonyl)guanidino]phenyl}ethanephosphonate

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Technology Process of diphenyl 1-amino-2-{4-[N,N'-bis(tert-butyloxycarbonyl)guanidino]phenyl}ethanephosphonate

There total 14 articles about diphenyl 1-amino-2-{4-[N,N'-bis(tert-butyloxycarbonyl)guanidino]phenyl}ethanephosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 695172-02-2
diphenyl 1-(benzyloxycarbonylamino)-2-{4-[N,N'-bis(tert-butyloxycarbonyl)guanidino]phenyl}ethanephosphonate

: 913239-29-9
diphenyl 1-amino-2-{4-[N,N'-bis(tert-butyloxycarbonyl)guanidino]phenyl}ethanephosphonate

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; at 20 ℃;
DOI:10.1021/jm700962j

Reference yield:

: 695172-02-2
diphenyl 1-benzyloxycarbonylamino-2-(4-(N,N'-bis(tert-butyloxycarbonyl)guanyl)phenyl)ethanephosphonate

: 913239-29-9
diphenyl 1-amino-2-(4-(N,N'-bis(tert-butyloxycarbonyl)guanidino)phenyl)ethyl-phosphonate

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; at 20 ℃; for 8h;
DOI:10.1021/jm0499209

Reference yield:

: 152120-54-2,862686-58-6,1143572-00-2
N,N'-bis( tert-butoxycarbonyl)-1H-pyrazole-1-carboxamidine

: 913239-29-9
diphenyl 1-amino-2-{4-[N,N'-bis(tert-butyloxycarbonyl)guanidino]phenyl}ethanephosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / acetonitrile / Heating

2: H₂ / Pd/C / methanol / 8 h / 20 °C

With hydrogen; triethylamine; palladium on activated charcoal; In methanol; acetonitrile;
DOI:10.1021/jm060622g