4-[N-[3-isopropyl-4-(methoxymethoxy)phenyl]-N-(3-methyl-2-butenyl)amino]-3,5-dimethylbenzaldehyde

Base Information

Chemical Name:4-[N-[3-isopropyl-4-(methoxymethoxy)phenyl]-N-(3-methyl-2-butenyl)amino]-3,5-dimethylbenzaldehyde
CAS No.:936133-27-6
Molecular Formula:C₂₅H₃₃NO₃
Molecular Weight:395.542
Hs Code.:

Synonyms:4-[N-[3-isopropyl-4-(methoxymethoxy)phenyl]-N-(3-methyl-2-butenyl)amino]-3,5-dimethylbenzaldehyde

Suppliers and Price of 4-[N-[3-isopropyl-4-(methoxymethoxy)phenyl]-N-(3-methyl-2-butenyl)amino]-3,5-dimethylbenzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-[N-[3-isopropyl-4-(methoxymethoxy)phenyl]-N-(3-methyl-2-butenyl)amino]-3,5-dimethylbenzaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-[N-[3-isopropyl-4-(methoxymethoxy)phenyl]-N-(3-methyl-2-butenyl)amino]-3,5-dimethylbenzaldehyde

There total 4 articles about 4-[N-[3-isopropyl-4-(methoxymethoxy)phenyl]-N-(3-methyl-2-butenyl)amino]-3,5-dimethylbenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 936133-22-1
4-[N-[3-isopropyl-4-(methoxymethoxy)phenyl]-N-(3-methyl-2-butenyl)amino]-3,5-dimethylbenzonitrile

: 936133-27-6
4-[N-[3-isopropyl-4-(methoxymethoxy)phenyl]-N-(3-methyl-2-butenyl)amino]-3,5-dimethylbenzaldehyde

Guidance literature:: With diisobutylaluminium hydride; In toluene; at 0 - 20 ℃;
DOI:10.1016/j.bmc.2007.02.053

Reference yield:

: 24596-19-8
4-bromo-2,6-dimethylphenylamine

: 936133-27-6
4-[N-[3-isopropyl-4-(methoxymethoxy)phenyl]-N-(3-methyl-2-butenyl)amino]-3,5-dimethylbenzaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: 76 percent / CuI; KI; N,N'-dimethylethylenediamine / dimethylformamide / 24 h / 100 °C

2: 76 percent / 2-(di-cyclohexylphosphino)biphenyl; t-BuONa / Pd₂(dba)3 / toluene / 19 h / 100 °C

3: 80 percent / NaH / dimethylformamide / 0 - 20 °C

4: 90 percent / diisobutylaluminium hydride / toluene / 0 - 20 °C

With copper(l) iodide; sodium hydride; diisobutylaluminium hydride; potassium iodide; sodium t-butanolate; N,N`-dimethylethylenediamine; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmc.2007.02.053

Reference yield:

: 74896-24-5
4-amino-3,5-dimethylbenzonitrile

: 936133-27-6
4-[N-[3-isopropyl-4-(methoxymethoxy)phenyl]-N-(3-methyl-2-butenyl)amino]-3,5-dimethylbenzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / 2-(di-cyclohexylphosphino)biphenyl; t-BuONa / Pd₂(dba)3 / toluene / 19 h / 100 °C

2: 80 percent / NaH / dimethylformamide / 0 - 20 °C

3: 90 percent / diisobutylaluminium hydride / toluene / 0 - 20 °C

With sodium hydride; diisobutylaluminium hydride; sodium t-butanolate; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmc.2007.02.053