C₄₄H₄₀O₇

Base Information

Chemical Name:C₄₄H₄₀O₇
CAS No.:1421313-17-8
Molecular Formula:C₄₄H₄₀O₇
Molecular Weight:680.797
Hs Code.:

C<sub>44</sub>H<sub>40</sub>O<sub>7</sub>

Synonyms:C₄₄H₄₀O₇

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Chemical Property of C₄₄H₄₀O₇

Chemical Property:

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Technology Process of C₄₄H₄₀O₇

There total 14 articles about C₄₄H₄₀O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₄H₃₈O₇

: 1421313-17-8
C₄₄H₄₀O₇

Guidance literature:: With aluminum isopropoxide; isopropyl alcohol; In toluene; for 1h; Inert atmosphere; Reflux;
DOI:10.1016/j.tetasy.2013.02.012

Reference yield:

: 100-44-7
benzyl chloride

: 1421313-17-8
C₄₄H₄₀O₇

Guidance literature:: Multi-step reaction with 10 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 35 - 65 °C / Inert atmosphere

1.2: 3 h / 65 - 70 °C / Inert atmosphere

2.1: sodium hydride / n-heptane; N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / Inert atmosphere

2.2: 2.17 h / 0 - 20 °C / Inert atmosphere

3.1: cerium(III) chloride heptahydrate; sodium tetrahydroborate / tetrahydrofuran; ethanol / 65 h / 2 °C / Inert atmosphere

3.2: Inert atmosphere

4.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

5.1: AD-mix-α; methanesulfonamide / tetrahydrofuran; water; tert-butyl alcohol / 96 h / -1 °C / Inert atmosphere

6.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

7.1: pyridinium p-toluenesulfonate / 1,2-dichloro-ethane / 1 h / 65 °C / Inert atmosphere

8.1: potassium carbonate; water / methanol / 24 h / 20 °C / Inert atmosphere

9.1: Dess-Martin periodane / dichloromethane / 3 h / 20 °C / Inert atmosphere

10.1: aluminum isopropoxide; isopropyl alcohol / toluene / 1 h / Inert atmosphere; Reflux

With 1H-imidazole; sodium tetrahydroborate; methanesulfonamide; cerium(III) chloride heptahydrate; AD-mix-α; tetrabutyl ammonium fluoride; water; pyridinium p-toluenesulfonate; aluminum isopropoxide; sodium hydride; potassium carbonate; Dess-Martin periodane; acetic acid; isopropyl alcohol; In tetrahydrofuran; methanol; ethanol; n-heptane; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene; mineral oil; tert-butyl alcohol; 2.1: |Aldol Condensation / 2.2: |Aldol Condensation / 5.1: |Sharpless Dihydroxylation;
DOI:10.1016/j.tetasy.2013.02.012

Reference yield:

: 1447605-67-5
C₄₄H₃₈O₇

: 1421313-17-8
C₄₄H₄₀O₇

Guidance literature:: Multi-step reaction with 8 steps

1.1: cerium(III) chloride heptahydrate; sodium tetrahydroborate / tetrahydrofuran; ethanol / 65 h / 2 °C / Inert atmosphere

1.2: Inert atmosphere

2.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

3.1: AD-mix-α; methanesulfonamide / tetrahydrofuran; water; tert-butyl alcohol / 96 h / -1 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

5.1: pyridinium p-toluenesulfonate / 1,2-dichloro-ethane / 1 h / 65 °C / Inert atmosphere

6.1: potassium carbonate; water / methanol / 24 h / 20 °C / Inert atmosphere

7.1: Dess-Martin periodane / dichloromethane / 3 h / 20 °C / Inert atmosphere

8.1: aluminum isopropoxide; isopropyl alcohol / toluene / 1 h / Inert atmosphere; Reflux

With 1H-imidazole; sodium tetrahydroborate; methanesulfonamide; cerium(III) chloride heptahydrate; AD-mix-α; tetrabutyl ammonium fluoride; water; pyridinium p-toluenesulfonate; aluminum isopropoxide; potassium carbonate; Dess-Martin periodane; acetic acid; isopropyl alcohol; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene; tert-butyl alcohol; 3.1: |Sharpless Dihydroxylation;
DOI:10.1016/j.tetasy.2013.02.012