C₅₂H₄₉N₁₃O₁₀S₆

Base Information

Chemical Name:C₅₂H₄₉N₁₃O₁₀S₆
CAS No.:924288-60-8
Molecular Formula:C₅₂H₄₉N₁₃O₁₀S₆
Molecular Weight:1208.44
Hs Code.:

C<sub>52</sub>H<sub>49</sub>N<sub>13</sub>O<sub>10</sub>S<sub>6</sub>

Synonyms:C₅₂H₄₉N₁₃O₁₀S₆

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Chemical Property of C₅₂H₄₉N₁₃O₁₀S₆

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Technology Process of C₅₂H₄₉N₁₃O₁₀S₆

There total 31 articles about C₅₂H₄₉N₁₃O₁₀S₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 924288-59-5
C₅₈H₆₃N₁₃O₁₀S₆Si

: 924288-60-8
C₅₂H₄₉N₁₃O₁₀S₆

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 25 ℃;
DOI:10.1002/anie.200602798

Reference yield:

: 2-tert-butoxycarbonylamino-3-(tert-butyl-dimethyl-silanyloxy)-3-phenyl-propionic acid

: 924288-60-8
C₅₂H₄₉N₁₃O₁₀S₆

Guidance literature:: Multi-step reaction with 13 steps

1.1: trifluoroacetic acid / H₂O / 1 h / 25 °C

1.2: 85 percent / HATU; i-Pr₂NEt / CH₂Cl₂ / 3 h / 25 °C

2.1: 82 percent / imidazole / dimethylformamide / 16 h / 25 °C

3.1: 80 percent / Lawesson reagent / benzene / 16 h / Heating

4.1: 92 percent / HF*pyridine; pyridine / tetrahydrofuran / 2 h / 25 °C

5.1: N,N-diethylaminosulfur trifluoride / CH₂Cl₂ / 1 h / -78 °C

6.1: BrCCl₃; 1,8-diazabicyclo[5.4.0]undec-7-ene / CH₂Cl₂ / 1 h / 0 °C

7.1: trifluoroacetic acid / CH₂Cl₂ / 1 h / 25 °C

8.1: HATU; i-Pr₂NEt / CH₂Cl₂ / 24 h / 25 °C

9.1: Me₃SnOH / 1,2-dichloro-ethane / 5 h / 80 °C

10.1: HATU; i-Pr₂NEt / CH₂Cl₂ / 16 h / 25 °C

11.1: 85 percent / N,N-diethylaminosulfur trifluoride / CH₂Cl₂ / 1 h / -25 °C

12.1: 80 percent / tetrabutylammonium fluoride / tetrahydrofuran / 25 °C

With Lawessons reagent; pyridine; 1H-imidazole; Bromotrichloromethane; diethylamino-sulfur trifluoride; tetrabutyl ammonium fluoride; pyridine hydrogenfluoride; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; trimethyltin(IV) hydroxide; trifluoroacetic acid; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In tetrahydrofuran; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; benzene;
DOI:10.1002/anie.200602798

Reference yield:

: 924288-30-2
4-{4-[3-amino-3,6-bis-(4-methoxycarbonyl-thiazol-2-yl)-2,3,4,5-tetrahydro-pyridin-2-yl]-thiazol-2-yl}-2,2-dimethyl-oxazolidine-3-carboxylic acid tert-butyl ester

: 924288-60-8
C₅₂H₄₉N₁₃O₁₀S₆

Guidance literature:: Multi-step reaction with 14 steps

1.1: 50 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / ethyl acetate / 5 h / Heating

2.1: trifluoroacetic acid / H₂O / 1 h / 25 °C

2.2: 85 percent / HATU; i-Pr₂NEt / CH₂Cl₂ / 3 h / 25 °C

3.1: 82 percent / imidazole / dimethylformamide / 16 h / 25 °C

4.1: 80 percent / Lawesson reagent / benzene / 16 h / Heating

5.1: 92 percent / HF*pyridine; pyridine / tetrahydrofuran / 2 h / 25 °C

6.1: N,N-diethylaminosulfur trifluoride / CH₂Cl₂ / 1 h / -78 °C

7.1: BrCCl₃; 1,8-diazabicyclo[5.4.0]undec-7-ene / CH₂Cl₂ / 1 h / 0 °C

8.1: trifluoroacetic acid / CH₂Cl₂ / 1 h / 25 °C

9.1: HATU; i-Pr₂NEt / CH₂Cl₂ / 24 h / 25 °C

10.1: Me₃SnOH / 1,2-dichloro-ethane / 5 h / 80 °C

11.1: HATU; i-Pr₂NEt / CH₂Cl₂ / 16 h / 25 °C

12.1: 85 percent / N,N-diethylaminosulfur trifluoride / CH₂Cl₂ / 1 h / -25 °C

13.1: 80 percent / tetrabutylammonium fluoride / tetrahydrofuran / 25 °C

With Lawessons reagent; pyridine; 1H-imidazole; Bromotrichloromethane; diethylamino-sulfur trifluoride; tetrabutyl ammonium fluoride; pyridine hydrogenfluoride; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; trimethyltin(IV) hydroxide; trifluoroacetic acid; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In tetrahydrofuran; dichloromethane; water; ethyl acetate; 1,2-dichloro-ethane; N,N-dimethyl-formamide; benzene;
DOI:10.1002/anie.200602798