METHYL 2-[4-(2-METHOXY-1-METHYL-2-OXOETHOXY)PHENOXY]PROPANOATE

Base Information

• Chemical Name: METHYL 2-[4-(2-METHOXY-1-METHYL-2-OXOETHOXY)PHENOXY]PROPANOATE
• CAS No.: 85977-51-1
• Molecular Formula: C₁₄H₁₈O₆
• Molecular Weight: 282.293
• Mol file: 85977-51-1.mol

Synonyms:2-[4-(1-Methoxycarbonyl-ethoxy)-phenoxy]-propionic acid methyl ester

Chemical Property of METHYL 2-[4-(2-METHOXY-1-METHYL-2-OXOETHOXY)PHENOXY]PROPANOATE

Chemical Property:

• Solubility.: Dichloromethane, Diethyl Ether, Ethyl Acetate; Methanol

Purity/Quality:

2,2''-[1,4-Phenylenebis(oxy)]bis-propanoicAcidDimethylEster ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: 2,2''-[1,4-Phenylenebis(oxy)]bis-propanoic Acid Dimethyl Ester is an intermediate in the synthesis of (±)-Fluazifop (F407430). (±)-Fluazifop is a grass-selective herbicide which inhibits acetyl-CoA carboxylase in sensitive plant species.

Technology Process of METHYL 2-[4-(2-METHOXY-1-METHYL-2-OXOETHOXY)PHENOXY]PROPANOATE

There total 1 articles about METHYL 2-[4-(2-METHOXY-1-METHYL-2-OXOETHOXY)PHENOXY]PROPANOATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.3%

2-chloro-propionic acid methyl ester (17639-93-9) + hydroquinone (123-31-9,8027-02-9) → 2-[4-(1-Methoxycarbonyl-ethoxy)-phenoxy]-propionic acid methyl ester (85977-51-1)

Guidance literature:

With disodium hydrogenphosphate; potassium carbonate; sodium iodide; In N,N-dimethyl-formamide; at 70 - 100 ℃; for 20h;

Reference yield: 38.8%

2-[4-(1-Methoxycarbonyl-ethoxy)-phenoxy]-propionic acid methyl ester (85977-51-1) → 2,2'-(1,4-phenylenebis(oxy))dipropionic acid (99967-54-1)

Guidance literature:

With hydrogenchloride; water; at 90 ℃; for 8h;

upstream raw materials:

2-chloro-propionic acid methyl ester

hydroquinone

Downstream raw materials:

2,2'-(1,4-phenylenebis(oxy))dipropionic acid

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