C₂₀H₃₅NOSi

Base Information

• Chemical Name: C₂₀H₃₅NOSi
• CAS No.: 943227-46-1
• Molecular Formula: C₂₀H₃₅NOSi
• Molecular Weight: 333.589
• Mol file: 943227-46-1.mol

Synonyms:C₂₀H₃₅NOSi

Chemical Property of C₂₀H₃₅NOSi

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₀H₃₅NOSi

There total 1 articles about C₂₀H₃₅NOSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

t-butyldimethylsiyl triflate (69739-34-0) + N-Benzyl-N-(1-isopropyl-but-3-enyl)-hydroxylamine (198694-24-5) → C20H35NOSi (943227-46-1)

Guidance literature:

With lutidine; In dichloromethane; at -40 - 20 ℃;

DOI:10.1055/s-2007-973868

Reference yield: 83.0%

C20H35NOSi (943227-46-1) + cis-1,4-bis(acetyloxy)but-2-ene (25260-60-0) → C23H39NO3Si (943227-65-4)

Guidance literature:

[1,3-bis-(2,4,6-trimethylphenyl)-2-imidazolidinylidene]dichloro(O-isopropoxyphenylmethylene)ruthenium; In dichloromethane; for 4h; Heating;

DOI:10.1055/s-2007-973868

Reference yield:

C20H35NOSi (943227-46-1) → C17H25NO3 (943227-78-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 83 percent / Hoveyda-Grubbs catalyst / CH₂Cl₂ / 4 h / Heating

2: 99 percent / TBAF / acetic acid

With tetrabutyl ammonium fluoride; [1,3-bis-(2,4,6-trimethylphenyl)-2-imidazolidinylidene]dichloro(O-isopropoxyphenylmethylene)ruthenium; In dichloromethane; acetic acid;

DOI:10.1055/s-2007-973868

upstream raw materials:

t-butyldimethylsiyl triflate

N-Benzyl-N-(1-isopropyl-but-3-enyl)-hydroxylamine

Downstream raw materials:

C₂₃H₃₉NO₃Si

C₁₇H₂₅NO₃