3-Cyclohexene-1-carboxamide, 1-methyl-

Base Information

• Chemical Name: 3-Cyclohexene-1-carboxamide, 1-methyl-
• CAS No.: 69352-89-2
• Molecular Formula: C8H13 N O
• Molecular Weight: 139.19
• DSSTox Substance ID: DTXSID60989089
• Nikkaji Number: J77.847H
• Mol file: 69352-89-2.mol

Synonyms:69352-89-2;3-Cyclohexene-1-carboxamide, 1-methyl-;1-methylcyclohex-3-ene-1-carboxamide;1-Methyl-3-cyclohexene-1-carboxamide;BRN 3237663;3-Cyclohexene-1-carboxamide,1-methyl-(7CI,9CI);1-Methylcyclohex-3-enecarboxamide;4-09-00-00126 (Beilstein Handbook Reference);SCHEMBL2128101;DTXSID60989089;QLTVNOWJTFRSSC-UHFFFAOYSA-N;MFCD01735000;AKOS006340371;AS-67057;LS-57418;1-Methylcyclohex-3-ene-1-carboximidic acid;CS-0036444;W12043;A1-01318

Chemical Property of 3-Cyclohexene-1-carboxamide, 1-methyl-

Chemical Property:

• Vapor Pressure: 0.00476mmHg at 25°C
• Boiling Point: 276.6°C at 760 mmHg
• Flash Point: 121.1°C
• PSA: 44.08000
• Density: 1.019g/cm³
• LogP: 2.36780
• XLogP3: 1
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 139.099714038
• Heavy Atom Count: 10
• Complexity: 174

Purity/Quality:

99% ^*data from raw suppliers

1-methylcyclohex-3-ene-1-carboxamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1(CCC=CC1)C(=O)N

Technology Process of 3-Cyclohexene-1-carboxamide, 1-methyl-

There total 4 articles about 3-Cyclohexene-1-carboxamide, 1-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-methyl-3-cyclohexenecarboxylic acid (16646-42-7) → 1-methylcyclohex-3-ene-1-carboxamide (69352-89-2)

Guidance literature:

With thionyl chloride; In dichloromethane; N,N-dimethyl-formamide; for 3h; Reflux;

Reference yield:

1,2,5,6-tetrahydrobenzoic acid (4771-80-6) → 1-methylcyclohex-3-ene-1-carboxamide (69352-89-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: N-ethyl-N,N-diisopropylamine; n-butyllithium / tetrahydrofuran; hexane / 2.5 h / -78 - 60 °C

1.2: 20 °C

2.1: thionyl chloride / N,N-dimethyl-formamide; dichloromethane / 3 h / Reflux

With n-butyllithium; thionyl chloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

→ 1-methylcyclohex-3-ene-1-carboxamide (69352-89-2)

Guidance literature:

With ammonium hydroxide;

upstream raw materials:

1,2,5,6-tetrahydrobenzoic acid

1-methyl-3-cyclohexenecarboxylic acid

Downstream raw materials:

tert butyl 4-iodo-1-methyl-7-oxo-6-azabicyclo[3.2.1]octane-6-carboxylate

methyl 5-(tert-butoxycarbonylamino)-1-methylcyclohex-3-enecarboxylate

methyl 5-(tert-butoxycarbonylamino)-1-methylcyclohexanecarboxylate

(1R,3S)-methyl 3-(2-chloro-5-fluoropyrimidin-4-ylamino)-1-methyl-cyclohexanecarboxylate

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 69352-89-2 3-Cyclohexene-1-carboxamide,1-methyl-(7CI,9CI)

Send

Send

Metric Ton KG G Pound L ML

Send

Send