diphenylmethyl 7β-(tritylamino)-3-(acetoxymethyl)-3-cephem-4-carboxylate 1-oxide

Base Information

Chemical Name:diphenylmethyl 7β-(tritylamino)-3-(acetoxymethyl)-3-cephem-4-carboxylate 1-oxide
CAS No.:90913-23-8
Molecular Formula:C₄₂H₃₆N₂O₆S
Molecular Weight:696.824
Hs Code.:

Synonyms:diphenylmethyl 7β-(tritylamino)-3-(acetoxymethyl)-3-cephem-4-carboxylate 1-oxide

Suppliers and Price of diphenylmethyl 7β-(tritylamino)-3-(acetoxymethyl)-3-cephem-4-carboxylate 1-oxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of diphenylmethyl 7β-(tritylamino)-3-(acetoxymethyl)-3-cephem-4-carboxylate 1-oxide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of diphenylmethyl 7β-(tritylamino)-3-(acetoxymethyl)-3-cephem-4-carboxylate 1-oxide

There total 4 articles about diphenylmethyl 7β-(tritylamino)-3-(acetoxymethyl)-3-cephem-4-carboxylate 1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (6R,7R)-3-Acetoxymethyl-8-oxo-7-(trityl-amino)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid benzhydryl ester

: 90913-23-8
diphenylmethyl 7β-(tritylamino)-3-(acetoxymethyl)-3-cephem-4-carboxylate 1-oxide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 5 ℃; for 1h;
DOI:10.1021/jm00375a026

Reference yield:

: 76-83-5
trityl chloride

: 90913-23-8
diphenylmethyl 7β-(tritylamino)-3-(acetoxymethyl)-3-cephem-4-carboxylate 1-oxide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Et₃N, dimethylaniline, 2.) trimethylsilyl chloride

2: CH₂Cl₂ / 1 h

3: 85percent m-chloroperbenzoic acid / CH₂Cl₂ / 1 h / 5 °C

With chloro-trimethyl-silane; triethylamine; 3-chloro-benzenecarboperoxoic acid; 2,3-Dimethylaniline; In dichloromethane;
DOI:10.1021/jm00375a026

Reference yield:

: 957-68-6
7-Aminocephalosporanic acid

: 90913-23-8
diphenylmethyl 7β-(tritylamino)-3-(acetoxymethyl)-3-cephem-4-carboxylate 1-oxide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Et₃N, dimethylaniline, 2.) trimethylsilyl chloride

2: CH₂Cl₂ / 1 h

3: 85percent m-chloroperbenzoic acid / CH₂Cl₂ / 1 h / 5 °C

With chloro-trimethyl-silane; triethylamine; 3-chloro-benzenecarboperoxoic acid; 2,3-Dimethylaniline; In dichloromethane;
DOI:10.1021/jm00375a026