2,6-Diallylphenol triflate

Base Information

• Chemical Name: 2,6-Diallylphenol triflate
• CAS No.: 311806-44-7
• Molecular Formula: C₁₃H₁₃F₃O₃S
• Molecular Weight: 306.306
• Mol file: 311806-44-7.mol

Synonyms:2,6-Diallylphenol triflate

Chemical Property of 2,6-Diallylphenol triflate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,6-Diallylphenol triflate

There total 1 articles about 2,6-Diallylphenol triflate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.9%

trifluoromethylsulfonic anhydride (358-23-6) + 2,6-diallylphenol (3382-99-8) → 2,6-Diallylphenol triflate (311806-44-7)

Guidance literature:

With pyridine; In dichloromethane; for 16h;

DOI:10.1039/b004525j

Reference yield: 47.9%

sodium diethyl phosphite (2303-76-6,118080-94-7) + 2,6-Diallylphenol triflate (311806-44-7) → Diethyl 2,6-diallylphenylphosphonate

Guidance literature:

sodium diethyl phosphite; 2,6-Diallylphenol triflate; In tetrahydrofuran; for 2h; Heating;

for 120h; Further stages.;

DOI:10.1039/b004525j

Reference yield:

2,6-Diallylphenol triflate (311806-44-7) → 2,6-diallylphenol (3382-99-8)

Guidance literature:

Multi-step reaction with 2 steps

1.1: tetrahydrofuran / 2 h / Heating

1.2: 47.9 percent / 120 h

2.1: LiAlH₄ / diethyl ether / 16 h / 20 °C

With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; 1.1: Substitution / 1.2: Rearrangement / 2.1: Reduction;

DOI:10.1039/b004525j

upstream raw materials:

trifluoromethylsulfonic anhydride

2,6-diallylphenol

Downstream raw materials:

2,6-diallylphenol

Refernces