tert-butyl (1S,2R)-3-azido-1-(3,5-difluorobenzyl)-2-hydroxypropylcarbamate

Base Information

Chemical Name:tert-butyl (1S,2R)-3-azido-1-(3,5-difluorobenzyl)-2-hydroxypropylcarbamate
CAS No.:388071-28-1
Molecular Formula:C₁₅H₂₀F₂N₄O₃
Molecular Weight:342.346
Hs Code.:

Synonyms:tert-butyl (1S,2R)-3-azido-1-(3,5-difluorobenzyl)-2-hydroxypropylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl (1S,2R)-3-azido-1-(3,5-difluorobenzyl)-2-hydroxypropylcarbamate

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Technology Process of tert-butyl (1S,2R)-3-azido-1-(3,5-difluorobenzyl)-2-hydroxypropylcarbamate

There total 1 articles about tert-butyl (1S,2R)-3-azido-1-(3,5-difluorobenzyl)-2-hydroxypropylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 881424-35-7
(1S,2S)-[1-(3,5-difluoro-benzyl)-2-hydroxy-3-iodo-propyl]-carbamic acid tert-butyl ester

: 388071-28-1
tert-butyl (1S,2R)-3-azido-1-(3,5-difluorobenzyl)-2-hydroxypropylcarbamate

Guidance literature:: (1S,2S)-[1-(3,5-difluoro-benzyl)-2-hydroxy-3-iodo-propyl]-carbamic acid tert-butyl ester; With potassium hydroxide; In ethanol; at 20 ℃;

With sodium azide; ammonium chloride; In water; isopropyl alcohol; at 60 ℃; for 8h; Further stages.;
DOI:10.1016/j.bmcl.2008.03.081

Reference yield: 92.0%

: 388071-28-1
tert-butyl (1S,2R)-3-azido-1-(3,5-difluorobenzyl)-2-hydroxypropylcarbamate

: 388075-52-3
((1S,2R)-3-amino-1-(3,5-difluorobenzyl)-2-hydroxy-propyl)carbamic acid t-butyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; at 20 ℃; for 4h; under 2327.23 Torr;
DOI:10.1016/j.bmcl.2008.03.081