N₁-[3-{[(4-bromo-2-chlorophenyl)sulfonyl]amino}-4-(methyloxy)phenyl]-2-methylalaninamide

Base Information

• Chemical Name: N₁-[3-{[(4-bromo-2-chlorophenyl)sulfonyl]amino}-4-(methyloxy)phenyl]-2-methylalaninamide
• CAS No.: 953391-75-8
• Molecular Formula: C₁₇H₁₉BrClN₃O₄S
• Molecular Weight: 476.779

Synonyms:N₁-[3-{[(4-bromo-2-chlorophenyl)sulfonyl]amino}-4-(methyloxy)phenyl]-2-methylalaninamide

Chemical Property of N₁-[3-{[(4-bromo-2-chlorophenyl)sulfonyl]amino}-4-(methyloxy)phenyl]-2-methylalaninamide

Chemical Property:

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Technology Process of N₁-[3-{[(4-bromo-2-chlorophenyl)sulfonyl]amino}-4-(methyloxy)phenyl]-2-methylalaninamide

There total 4 articles about N₁-[3-{[(4-bromo-2-chlorophenyl)sulfonyl]amino}-4-(methyloxy)phenyl]-2-methylalaninamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-[5-amino-2-(methyloxy)phenyl]-4-bromo-2-chlorobenzenesulfonamide (953391-74-7) + 2-amino-2-methylpropanoyl chloride (78002-19-4) → N1-[3-{[(4-bromo-2-chlorophenyl)sulfonyl]amino}-4-(methyloxy)phenyl]-2-methylalaninamide (953391-75-8)

Guidance literature:

With pyridine; In dichloromethane; at 20 ℃;

Reference yield:

4-bromo-2-chloro-N-[2-(methyloxy)-5-nitrophenyl]benzenesulfonamide (953391-73-6) → N1-[3-{[(4-bromo-2-chlorophenyl)sulfonyl]amino}-4-(methyloxy)phenyl]-2-methylalaninamide (953391-75-8)

Guidance literature:

Multi-step reaction with 2 steps

1: ammonium formate / 5 % platinum on carbon / methanol; water / 40 h / 20 °C

2: pyridine / dichloromethane / 20 °C

With pyridine; ammonium formate; 5 % platinum on carbon; In methanol; dichloromethane; water;

Reference yield:

3-amino-4-methoxynitrobenzene (99-59-2) → N1-[3-{[(4-bromo-2-chlorophenyl)sulfonyl]amino}-4-(methyloxy)phenyl]-2-methylalaninamide (953391-75-8)

Guidance literature:

Multi-step reaction with 3 steps

1: pyridine / dichloromethane / 20 °C

2: ammonium formate / 5 % platinum on carbon / methanol; water / 40 h / 20 °C

3: pyridine / dichloromethane / 20 °C

With pyridine; ammonium formate; 5 % platinum on carbon; In methanol; dichloromethane; water;

upstream raw materials:

N-[5-amino-2-(methyloxy)phenyl]-4-bromo-2-chlorobenzenesulfonamide

2-amino-2-methylpropanoyl chloride

4-bromo-2-chloro-N-[2-(methyloxy)-5-nitrophenyl]benzenesulfonamide

4-bromo-2-chlorobenzene-1-sulfonyl chloride

Downstream raw materials:

N₁-[3-({[2-chloro-4-(5-methyl-2-furanyl)phenyl]sulfonyl}amino)-4-(methyloxy)phenyl]-2-methylalaninamide hydrochloride

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