Technology Process of C46H53NO13
There total 6 articles about C46H53NO13 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine; hydrogen fluoride;
In
tetrahydrofuran;
at 20 ℃;
DOI:10.1002/ejoc.200500243
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: methanol / 17 h / 20 °C
1.2: methanol / 48 h / Heating
2.1: K2621 Bayer catalyst / CH2Cl2 / 21 h
2.2: 16 percent / NaH / acetonitrile / 20 h / 20 °C
3.1: 68 percent / sodium hydroxyde / H2O; tetrahydrofuran / 22 h / ambient temperature
4.1: 34 percent / DCC; 4-PP / toluene / 24 h / 20 °C
5.1: 98 percent / pyridine; HF / tetrahydrofuran / 20 °C
With
pyridine; sodium hydroxide; K2621 Bayer catalyst; hydrogen fluoride; dicyclohexyl-carbodiimide;
In
tetrahydrofuran; methanol; dichloromethane; water; toluene;
DOI:10.1002/ejoc.200500243
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: K2621 Bayer catalyst / CH2Cl2 / 21 h
1.2: 16 percent / NaH / acetonitrile / 20 h / 20 °C
2.1: 68 percent / sodium hydroxyde / H2O; tetrahydrofuran / 22 h / ambient temperature
3.1: 34 percent / DCC; 4-PP / toluene / 24 h / 20 °C
4.1: 98 percent / pyridine; HF / tetrahydrofuran / 20 °C
With
pyridine; sodium hydroxide; K2621 Bayer catalyst; hydrogen fluoride; dicyclohexyl-carbodiimide;
In
tetrahydrofuran; dichloromethane; water; toluene;
DOI:10.1002/ejoc.200500243
