1-(2,6-Dimethoxy-4-pentyl-phenyl)-6-(1-methoxy-1-methyl-ethyl)-cyclohex-2-enol

Base Information

Chemical Name:1-(2,6-Dimethoxy-4-pentyl-phenyl)-6-(1-methoxy-1-methyl-ethyl)-cyclohex-2-enol
CAS No.:122700-18-9
Molecular Formula:C₂₃H₃₆O₄
Molecular Weight:376.536
Hs Code.:

Synonyms:1-(2,6-Dimethoxy-4-pentyl-phenyl)-6-(1-methoxy-1-methyl-ethyl)-cyclohex-2-enol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(2,6-Dimethoxy-4-pentyl-phenyl)-6-(1-methoxy-1-methyl-ethyl)-cyclohex-2-enol

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Technology Process of 1-(2,6-Dimethoxy-4-pentyl-phenyl)-6-(1-methoxy-1-methyl-ethyl)-cyclohex-2-enol

There total 1 articles about 1-(2,6-Dimethoxy-4-pentyl-phenyl)-6-(1-methoxy-1-methyl-ethyl)-cyclohex-2-enol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 122700-11-2
6-(1-Methoxy-1-methylethyl)-2-cyclohexen-1-one

: 67895-00-5
(2,6-dimethoxy-4-pentylphenyl)lithium

: 122700-18-9
1-(2,6-Dimethoxy-4-pentyl-phenyl)-6-(1-methoxy-1-methyl-ethyl)-cyclohex-2-enol

Guidance literature:: In tetrahydrofuran; for 4h; Heating;
DOI:10.1021/jo00281a009

Reference yield:

: 122700-18-9
1-(2,6-Dimethoxy-4-pentyl-phenyl)-6-(1-methoxy-1-methyl-ethyl)-cyclohex-2-enol

: 122700-12-3
3-(2,6-Dimethoxy-4-pentyl-phenyl)-4-(1-methoxy-1-methyl-ethyl)-cyclohex-2-enone

Guidance literature:: With jones reagent; In acetone; at 0 - 25 ℃; for 0.5h; Yield given;
DOI:10.1021/jo00281a009

Reference yield:

: 122700-18-9
1-(2,6-Dimethoxy-4-pentyl-phenyl)-6-(1-methoxy-1-methyl-ethyl)-cyclohex-2-enol

: 16849-41-5,6469-58-5
1-Hydroxy-3-pentyl-6,6a,7,8-tetrahydro-6,6-dimethyl-9H-dibenzopyran-9-one

Guidance literature:: Multi-step reaction with 2 steps

1: Jones reagent / acetone / 0.5 h / 0 - 25 °C

2: BBr₃ / CH₂Cl₂ / 6 h / -78 - 25 °C

With jones reagent; boron tribromide; In dichloromethane; acetone;
DOI:10.1021/jo00281a009