2-(2-Adamantan-1-yl-1-benzenesulfonyl-1-trimethylsilanyl-ethylsulfanyl)-pyridine

Base Information

• Chemical Name: 2-(2-Adamantan-1-yl-1-benzenesulfonyl-1-trimethylsilanyl-ethylsulfanyl)-pyridine
• CAS No.: 135967-11-2
• Molecular Formula: C₂₆H₃₅NO₂S₂Si
• Molecular Weight: 485.787

Synonyms:2-(2-Adamantan-1-yl-1-benzenesulfonyl-1-trimethylsilanyl-ethylsulfanyl)-pyridine

Chemical Property of 2-(2-Adamantan-1-yl-1-benzenesulfonyl-1-trimethylsilanyl-ethylsulfanyl)-pyridine

Chemical Property:

Purity/Quality:

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Technology Process of 2-(2-Adamantan-1-yl-1-benzenesulfonyl-1-trimethylsilanyl-ethylsulfanyl)-pyridine

There total 1 articles about 2-(2-Adamantan-1-yl-1-benzenesulfonyl-1-trimethylsilanyl-ethylsulfanyl)-pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(adamantane-1-carbonyloxy)pyridine-2(1H)-thione (91233-19-1) + 1-(phenylsulfonyl)-1-(trimethylsilyl)ethene (69627-08-3) → 2-(2-Adamantan-1-yl-1-benzenesulfonyl-1-trimethylsilanyl-ethylsulfanyl)-pyridine (135967-11-2)

Guidance literature:

In dichloromethane; at 0 - 5 ℃;

DOI:10.1016/S0040-4039(00)92693-5

Reference yield:

2-(2-Adamantan-1-yl-1-benzenesulfonyl-1-trimethylsilanyl-ethylsulfanyl)-pyridine (135967-11-2) → (adamant-1-yl)-acetic acid (4942-47-6)

Guidance literature:

Multi-step reaction with 2 steps

1: m-chloroperbenzoic acid

2: 1) CF₃CO₂H 2) K₂CO₃ / 2) MeCN, H₂O

With potassium carbonate; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid;

DOI:10.1016/S0040-4039(00)92693-5

Reference yield:

2-(2-Adamantan-1-yl-1-benzenesulfonyl-1-trimethylsilanyl-ethylsulfanyl)-pyridine (135967-11-2) → 2-(2-Adamantan-1-yl-1-benzenesulfonyl-1-trimethylsilanyl-ethanesulfinyl)-pyridine (135967-17-8)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid;

DOI:10.1016/S0040-4039(00)92693-5

upstream raw materials:

1-(adamantane-1-carbonyloxy)pyridine-2(1H)-thione

1-(phenylsulfonyl)-1-(trimethylsilyl)ethene

Downstream raw materials:

2-(2-Adamantan-1-yl-1-benzenesulfonyl-1-trimethylsilanyl-ethanesulfinyl)-pyridine

(adamant-1-yl)-acetic acid

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