5-<oxy>-2'-methoxybiphenyl-2-yl phenyl ketone

Base Information

Chemical Name:5-<oxy>-2'-methoxybiphenyl-2-yl phenyl ketone
CAS No.:133721-64-9
Molecular Formula:C₂₈H₃₄O₃Si
Molecular Weight:446.662
Hs Code.:

5-<<Dimethyl(1,1,2-trimethylpropyl)silyl>oxy>-2'-methoxybiphenyl-2-yl phenyl ketone

Synonyms:5-<oxy>-2'-methoxybiphenyl-2-yl phenyl ketone

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Chemical Property of 5-<oxy>-2'-methoxybiphenyl-2-yl phenyl ketone

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Technology Process of 5-<oxy>-2'-methoxybiphenyl-2-yl phenyl ketone

There total 4 articles about 5-<oxy>-2'-methoxybiphenyl-2-yl phenyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.5%

: 103588-79-0
(1,1,2,2-tetramethyleth-1-yl)-dimethylsilyl trifluoromethanesulfonate

: 133721-53-6
2,3-Dihydro-2,2-dimethyl-6-(2-methoxyphenyl)-4H-pyran-4-one

: 3623-15-2
phenyl propargyl ketone

: 133721-64-9
5-<oxy>-2'-methoxybiphenyl-2-yl phenyl ketone

Guidance literature:: With di(tert-butyl)pyridine; In chloroform; 1.) 0 deg C, 2 h, 2.) r.t., 2 h;
DOI:10.1002/hlca.19910740106

Reference yield:

: 133721-46-7
5-Hydroxy-1-(2-methoxyphenyl)-5-methylhex-2-yn-1-one

: 133721-64-9
5-<oxy>-2'-methoxybiphenyl-2-yl phenyl ketone

Guidance literature:: Multi-step reaction with 2 steps

1: 96.3 percent / 33 percent HBr/AcOH / CH₂Cl₂ / 1.) 0 deg C, 30 min, 2.) r.t., 4-10 h

2: 87.5 percent / di(tert-butyl)pyridine / CHCl₃ / 1.) 0 deg C, 2 h, 2.) r.t., 2 h

With di(tert-butyl)pyridine; hydrogen bromide; acetic acid; In dichloromethane; chloroform;
DOI:10.1002/hlca.19910740106

Reference yield:

: 1-(2-Methoxy-phenyl)-5-methyl-hex-2-yne-1,5-diol

: 133721-64-9
5-<oxy>-2'-methoxybiphenyl-2-yl phenyl ketone

Guidance literature:: Multi-step reaction with 3 steps

1: MnO₂ / CH₂Cl₂ / 1.) 0 deg C, 1 h, 2.) r.t., 30 min

2: 96.3 percent / 33 percent HBr/AcOH / CH₂Cl₂ / 1.) 0 deg C, 30 min, 2.) r.t., 4-10 h

3: 87.5 percent / di(tert-butyl)pyridine / CHCl₃ / 1.) 0 deg C, 2 h, 2.) r.t., 2 h

With manganese(IV) oxide; di(tert-butyl)pyridine; hydrogen bromide; acetic acid; In dichloromethane; chloroform;
DOI:10.1002/hlca.19910740106