2,6-anhydro-N-benzyl-3-deoxy-4,5:7,8-di-O-isopropylidene-D-glycero-D-talo-octonamide

Base Information

Chemical Name:2,6-anhydro-N-benzyl-3-deoxy-4,5:7,8-di-O-isopropylidene-D-glycero-D-talo-octonamide
CAS No.:114474-91-8
Molecular Formula:C₂₁H₂₉NO₆
Molecular Weight:391.464
Hs Code.:

Synonyms:2,6-anhydro-N-benzyl-3-deoxy-4,5:7,8-di-O-isopropylidene-D-glycero-D-talo-octonamide

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Chemical Property of 2,6-anhydro-N-benzyl-3-deoxy-4,5:7,8-di-O-isopropylidene-D-glycero-D-talo-octonamide

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Technology Process of 2,6-anhydro-N-benzyl-3-deoxy-4,5:7,8-di-O-isopropylidene-D-glycero-D-talo-octonamide

There total 2 articles about 2,6-anhydro-N-benzyl-3-deoxy-4,5:7,8-di-O-isopropylidene-D-glycero-D-talo-octonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109150-74-5
methyl [2R,3S,4R,6S,1'R]-3,4-isopropylidenedioxy-2-[(1,2-isopropylidenedioxy)ethyl]tetrahydroo-2H-pyran-6-carboxylate

: 114474-91-8
2,6-anhydro-N-benzyl-3-deoxy-4,5:7,8-di-O-isopropylidene-D-glycero-D-talo-octonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / 2M NaOH / H₂O / 2 h / Ambient temperature

2: 1.) triethylamine, ethyl chloroformate; 2.) triethylamine / 1.) acetonitrile, -10 deg C, 5 min; 2.) acetonitrile, 1 h

With sodium hydroxide; chloroformic acid ethyl ester; triethylamine; In water;
DOI:10.1016/0008-6215(87)80060-5

Reference yield:

: 114474-87-2
(3aR,4R,6S,7aR)-4-((R)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-6-carboxylic acid; compound with triethyl-amine

: 100-46-9
benzylamine

: 114474-91-8
2,6-anhydro-N-benzyl-3-deoxy-4,5:7,8-di-O-isopropylidene-D-glycero-D-talo-octonamide

Guidance literature:: With chloroformic acid ethyl ester; triethylamine; Yield given. Multistep reaction; 1.) acetonitrile, -10 deg C, 5 min; 2.) acetonitrile, 1 h;
DOI:10.1016/0008-6215(87)80060-5