(S)-2-[3-(4-{2-[(S)-2-(tert-Butyl-dimethyl-silanyloxymethyl)-pyrrolidine-1-carbonyl]-4,5-dimethoxy-phenylcarbamoyloxymethyl}-phenyl)-ureido]-pentanedioic acid diallyl ester

Base Information

Chemical Name:(S)-2-[3-(4-{2-[(S)-2-(tert-Butyl-dimethyl-silanyloxymethyl)-pyrrolidine-1-carbonyl]-4,5-dimethoxy-phenylcarbamoyloxymethyl}-phenyl)-ureido]-pentanedioic acid diallyl ester
CAS No.:848004-44-4
Molecular Formula:C₄₀H₅₆N₄O₁₁Si
Molecular Weight:796.99
Hs Code.:

(S)-2-[3-(4-{2-[(S)-2-(tert-Butyl-dimethyl-silanyloxymethyl)-pyrrolidine-1-carbonyl]-4,5-dimethoxy-phenylcarbamoyloxymethyl}-phenyl)-ureido]-pentanedioic acid diallyl ester

Synonyms:(S)-2-[3-(4-{2-[(S)-2-(tert-Butyl-dimethyl-silanyloxymethyl)-pyrrolidine-1-carbonyl]-4,5-dimethoxy-phenylcarbamoyloxymethyl}-phenyl)-ureido]-pentanedioic acid diallyl ester

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Chemical Property of (S)-2-[3-(4-{2-[(S)-2-(tert-Butyl-dimethyl-silanyloxymethyl)-pyrrolidine-1-carbonyl]-4,5-dimethoxy-phenylcarbamoyloxymethyl}-phenyl)-ureido]-pentanedioic acid diallyl ester

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Technology Process of (S)-2-[3-(4-{2-[(S)-2-(tert-Butyl-dimethyl-silanyloxymethyl)-pyrrolidine-1-carbonyl]-4,5-dimethoxy-phenylcarbamoyloxymethyl}-phenyl)-ureido]-pentanedioic acid diallyl ester

There total 3 articles about (S)-2-[3-(4-{2-[(S)-2-(tert-Butyl-dimethyl-silanyloxymethyl)-pyrrolidine-1-carbonyl]-4,5-dimethoxy-phenylcarbamoyloxymethyl}-phenyl)-ureido]-pentanedioic acid diallyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 848004-21-7
[2-(tert-butyl-dimethyl-silanyloxymethyl)-pyrrolidin-1-yl]-(2-isocyanato-4,5-dimethoxy-phenyl)-methanone

: 32315-10-9
bis(trichloromethyl) carbonate

: 180839-13-8
diprop-2-enyl N-<(4-phenyl)carbamoyl>-L-glutamate

: 848004-44-4
(S)-2-[3-(4-{2-[(S)-2-(tert-Butyl-dimethyl-silanyloxymethyl)-pyrrolidine-1-carbonyl]-4,5-dimethoxy-phenylcarbamoyloxymethyl}-phenyl)-ureido]-pentanedioic acid diallyl ester

Guidance literature:: With triethylamine; In toluene; for 20h;

Reference yield:

: 848004-21-7
[2-(tert-butyl-dimethyl-silanyloxymethyl)-pyrrolidin-1-yl]-(2-isocyanato-4,5-dimethoxy-phenyl)-methanone

: 180839-13-8
diprop-2-enyl N-<(4-phenyl)carbamoyl>-L-glutamate

: 848004-44-4
(S)-2-[3-(4-{2-[(S)-2-(tert-Butyl-dimethyl-silanyloxymethyl)-pyrrolidine-1-carbonyl]-4,5-dimethoxy-phenylcarbamoyloxymethyl}-phenyl)-ureido]-pentanedioic acid diallyl ester

Guidance literature:: With TEA; In dichloromethane; at 20 ℃; for 18h;
DOI:10.1016/j.bmcl.2005.10.017

Reference yield:

: 848004-19-3
(2-amino-4,5-dimethoxy-phenyl)-[2-(tert-butyl-dimethyl-silanyloxymethyl)-pyrrolidin-1-yl]-methanone

: 848004-44-4
(S)-2-[3-(4-{2-[(S)-2-(tert-Butyl-dimethyl-silanyloxymethyl)-pyrrolidine-1-carbonyl]-4,5-dimethoxy-phenylcarbamoyloxymethyl}-phenyl)-ureido]-pentanedioic acid diallyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: TEA / toluene / 2 h / 20 °C

2: TEA / CH₂Cl₂ / 18 h / 20 °C

With TEA; In dichloromethane; toluene;
DOI:10.1016/j.bmcl.2005.10.017