Fmoc-cis-Hyp(O-3,5-dinitrobenzoate)-O-Allyl

Base Information

Chemical Name:Fmoc-cis-Hyp(O-3,5-dinitrobenzoate)-O-Allyl
CAS No.:853245-47-3
Molecular Formula:C₃₀H₂₅N₃O₁₀
Molecular Weight:587.543
Hs Code.:

Synonyms:Fmoc-cis-Hyp(O-3,5-dinitrobenzoate)-O-Allyl

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Fmoc-cis-Hyp(O-3,5-dinitrobenzoate)-O-Allyl

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Technology Process of Fmoc-cis-Hyp(O-3,5-dinitrobenzoate)-O-Allyl

There total 2 articles about Fmoc-cis-Hyp(O-3,5-dinitrobenzoate)-O-Allyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 99-34-3
3,5-dinitrobenzoic acid

: 468096-64-2
4-hydroxypyrrolidine-1,2-dicarboxylic acid 2-allyl ester 1-(9H-fluoren-9-ylmethyl) ester

: 853245-47-3
Fmoc-cis-Hyp(O-3,5-dinitrobenzoate)-O-Allyl

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; toluene; at 0 - 20 ℃; for 22h;
DOI:10.1002/anie.200700017

Reference yield:

: 88050-17-3
N-Fmoc-trans-4-Hydroxy-L-Proline

: 853245-47-3
Fmoc-cis-Hyp(O-3,5-dinitrobenzoate)-O-Allyl

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / Cs₂CO₃ / dimethylformamide / 20 h / 20 °C

2: 80 percent / triphenylphosphine; di-tert-butyl azodicarboxylate / tetrahydrofuran; toluene / 16 h / 20 °C

With di-tert-butyl-diazodicarboxylate; caesium carbonate; triphenylphosphine; In tetrahydrofuran; N,N-dimethyl-formamide; toluene; 2: Mitsunobu reaction;
DOI:10.1021/jo0503153