(2R,3S)-3-<(tert-butyloxycarbonyl)amino>-1-(phenylsulfonyl)-2-hydroxy-5-methylhexane

Base Information

Chemical Name:(2R,3S)-3-<(tert-butyloxycarbonyl)amino>-1-(phenylsulfonyl)-2-hydroxy-5-methylhexane
CAS No.:109996-70-5
Molecular Formula:C₁₈H₂₉NO₅S
Molecular Weight:371.498
Hs Code.:

Synonyms:(2R,3S)-3-<(tert-butyloxycarbonyl)amino>-1-(phenylsulfonyl)-2-hydroxy-5-methylhexane

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Chemical Property of (2R,3S)-3-<(tert-butyloxycarbonyl)amino>-1-(phenylsulfonyl)-2-hydroxy-5-methylhexane

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Technology Process of (2R,3S)-3-<(tert-butyloxycarbonyl)amino>-1-(phenylsulfonyl)-2-hydroxy-5-methylhexane

There total 5 articles about (2R,3S)-3-<(tert-butyloxycarbonyl)amino>-1-(phenylsulfonyl)-2-hydroxy-5-methylhexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 109996-54-5
(2R,3S)-3-<(tert-butyloxycarbonyl)amino>-1-(phenylthio)-2-hydroxy-5-methylhexane

: 109996-70-5
(2R,3S)-3-<(tert-butyloxycarbonyl)amino>-1-(phenylsulfonyl)-2-hydroxy-5-methylhexane

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/jm00392a015

Reference yield:

: (3S)-3-(tert-butoxycarbonylamino)-5-methyl-1-(phenylsulfonyl)-2-hexanone

: 109996-70-5
(2R,3S)-3-<(tert-butyloxycarbonyl)amino>-1-(phenylsulfonyl)-2-hydroxy-5-methylhexane

: 799560-34-2
(2S,3S)-3-(tert-butoxycarbonylamino)-5-methyl-1-phenylsulfonyl-2-hexanol

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 ℃;
DOI:10.3390/molecules21060805

Reference yield:

: 108-98-5
thiophenol

: 109996-70-5
(2R,3S)-3-<(tert-butyloxycarbonyl)amino>-1-(phenylsulfonyl)-2-hydroxy-5-methylhexane

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / Et₃N / methanol / 2 h / Heating

2: 68 percent / 3-chloroperoxybenzoic acid (MCPBA) / CH₂Cl₂

With triethylamine; 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane;
DOI:10.1021/jm00392a015