4-((3,7-dimethyl-1H-dipyrazolo[5,1-c:3',4'-e][1,2,4]triazin-6-yl)diazenyl)-1,5-dimethyl-2-phenyl-1H-pyrazol-3(2H)-one

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Chemical Name:4-((3,7-dimethyl-1H-dipyrazolo[5,1-c:3',4'-e][1,2,4]triazin-6-yl)diazenyl)-1,5-dimethyl-2-phenyl-1H-pyrazol-3(2H)-one
CAS No.:1414859-86-1
Molecular Formula:C₁₉H₁₈N₁₀O
Molecular Weight:402.418
Hs Code.:

Synonyms:4-((3,7-dimethyl-1H-dipyrazolo[5,1-c:3',4'-e][1,2,4]triazin-6-yl)diazenyl)-1,5-dimethyl-2-phenyl-1H-pyrazol-3(2H)-one

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Chemical Property of 4-((3,7-dimethyl-1H-dipyrazolo[5,1-c:3',4'-e][1,2,4]triazin-6-yl)diazenyl)-1,5-dimethyl-2-phenyl-1H-pyrazol-3(2H)-one

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Technology Process of 4-((3,7-dimethyl-1H-dipyrazolo[5,1-c:3',4'-e][1,2,4]triazin-6-yl)diazenyl)-1,5-dimethyl-2-phenyl-1H-pyrazol-3(2H)-one

There total 4 articles about 4-((3,7-dimethyl-1H-dipyrazolo[5,1-c:3',4'-e][1,2,4]triazin-6-yl)diazenyl)-1,5-dimethyl-2-phenyl-1H-pyrazol-3(2H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1414859-85-0
1,5-dimethyl-4-((E)-(5-methyl-3-((E)-2-(3-methyl-5-oxo-1H-pyrazol-4(5H)-ylidene)hydrazinyl)-1H-pyrazol-4-yl)diazenyl)-2-phenyl-1H-pyrazol-3(2H)-one

: 1414859-86-1
4-((3,7-dimethyl-1H-dipyrazolo[5,1-c:3',4'-e][1,2,4]triazin-6-yl)diazenyl)-1,5-dimethyl-2-phenyl-1H-pyrazol-3(2H)-one

Guidance literature:: With trichlorophosphate; In N,N-dimethyl-formamide; for 12h; Reflux;
DOI:10.1016/j.ejmech.2012.08.034

Reference yield:

: 82315-71-7
N'-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-2-iminopropanehydrazonoyl cyanide

: 1414859-86-1
4-((3,7-dimethyl-1H-dipyrazolo[5,1-c:3',4'-e][1,2,4]triazin-6-yl)diazenyl)-1,5-dimethyl-2-phenyl-1H-pyrazol-3(2H)-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrazine hydrate / 1,4-dioxane / 4 h / Reflux

2.1: hydrogenchloride; sodium nitrite; acetic acid / water / Cooling with ice

2.2: 2 h

3.1: trichlorophosphate / N,N-dimethyl-formamide / 12 h / Reflux

With hydrogenchloride; hydrazine hydrate; acetic acid; sodium nitrite; trichlorophosphate; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.08.034

Reference yield:

: 83-07-8
4-amino-2,3-dimethyl-1-phenylpyrazolin-5-one

: 1414859-86-1
4-((3,7-dimethyl-1H-dipyrazolo[5,1-c:3',4'-e][1,2,4]triazin-6-yl)diazenyl)-1,5-dimethyl-2-phenyl-1H-pyrazol-3(2H)-one

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride; sodium nitrite / water / Cooling with ice

1.2: 2 h

2.1: hydrazine hydrate / 1,4-dioxane / 4 h / Reflux

3.1: hydrogenchloride; sodium nitrite; acetic acid / water / Cooling with ice

3.2: 2 h

4.1: trichlorophosphate / N,N-dimethyl-formamide / 12 h / Reflux

With hydrogenchloride; hydrazine hydrate; acetic acid; sodium nitrite; trichlorophosphate; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.08.034