Technology Process of C70H85ClN6O9
There total 6 articles about C70H85ClN6O9 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
thionyl chloride;
In
dichloromethane;
at 0 - 20 ℃;
Inert atmosphere;
DOI:10.1021/ja5041573
- Guidance literature:
-
Multi-step reaction with 4 steps
1: phosphorus tribromide / N,N-dimethyl-formamide; dichloromethane; tetrahydrofuran / 20 °C / Inert atmosphere
2: potassium carbonate / N,N-dimethyl-formamide / 12 h / 70 °C / Inert atmosphere
3: lithium aluminium tetrahydride / tetrahydrofuran / 20 °C / Inert atmosphere
4: thionyl chloride / dichloromethane / 0 - 20 °C / Inert atmosphere
With
lithium aluminium tetrahydride; thionyl chloride; phosphorus tribromide; potassium carbonate;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja5041573
- Guidance literature:
-
Multi-step reaction with 2 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 20 °C / Inert atmosphere
2: thionyl chloride / dichloromethane / 0 - 20 °C / Inert atmosphere
With
lithium aluminium tetrahydride; thionyl chloride;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/ja5041573