C₄₅H₇₅F₇O₃Si₃

Base Information

Chemical Name:C₄₅H₇₅F₇O₃Si₃
CAS No.:910624-36-1
Molecular Formula:C₄₅H₇₅F₇O₃Si₃
Molecular Weight:881.334
Hs Code.:

C<sub>45</sub>H<sub>75</sub>F<sub>7</sub>O<sub>3</sub>Si<sub>3</sub>

Synonyms:C₄₅H₇₅F₇O₃Si₃

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Chemical Property of C₄₅H₇₅F₇O₃Si₃

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Technology Process of C₄₅H₇₅F₇O₃Si₃

There total 21 articles about C₄₅H₇₅F₇O₃Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 910623-89-1
(1R,3aR,4S,7aR)-7a-methyl-1-[(1R)-6,6,6-trifluoro-1-methyl-1-(4-methyl-4-trimethylsilanyloxy-pentyl)-5-trifluoromethyl-5-trimethylsilanyloxy-hex-3-ynyl]-octahydro-inden-4-one

: 910624-36-1
C₄₅H₇₅F₇O₃Si₃

Guidance literature:: <3S-(1Z,3α,5β)>-<2-<3-Fluoro-5-<<(1,1-dimethylethyl)dimethylsilyl>oxy>-2-methylenecyclohexylidene>ethyl>diphenylphosphine Oxide; With n-butyllithium; In tetrahydrofuran; at -70 ℃; for 0.333333h;

(1R,3aR,4S,7aR)-7a-methyl-1-[(1R)-6,6,6-trifluoro-1-methyl-1-(4-methyl-4-trimethylsilanyloxy-pentyl)-5-trifluoromethyl-5-trimethylsilanyloxy-hex-3-ynyl]-octahydro-inden-4-one; In tetrahydrofuran; at -40 ℃; for 6h;

Reference yield:

: 910623-89-1
(1R,3aR,4S,7aR)-7a-methyl-1-[(1R)-6,6,6-trifluoro-1-methyl-1-(4-methyl-4-trimethylsilanyloxy-pentyl)-5-trifluoromethyl-5-trimethylsilanyloxy-hex-3-ynyl]-octahydro-inden-4-one

: 123836-63-5
<3S-(1Z,3α,5β)>-<2-<3-Fluoro-5-<<(1,1-dimethylethyl)dimethylsilyl>oxy>-2-methylenecyclohexylidene>ethyl>diphenylphosphine Oxide

: 910624-36-1
C₄₅H₇₅F₇O₃Si₃

Guidance literature:: <3S-(1Z,3α,5β)>-<2-<3-Fluoro-5-<<(1,1-dimethylethyl)dimethylsilyl>oxy>-2-methylenecyclohexylidene>ethyl>diphenylphosphine Oxide; With n-butyllithium; at -70 ℃; for 0.333333h;

(1R,3aR,4S,7aR)-7a-methyl-1-[(1R)-6,6,6-trifluoro-1-methyl-1-(4-methyl-4-trimethylsilanyloxy-pentyl)-5-trifluoromethyl-5-trimethylsilanyloxy-hex-3-ynyl]-octahydro-inden-4-one; In tetrahydrofuran; for 4.5h;

Reference yield:

: 1014717-75-9
(S,Z)-tert-butyl(2-(5-((tert-butyldimethylsilyl)oxy)-2-methylenecyclohexylidene)ethoxy)dimethylsilane

: 910624-36-1
C₄₅H₇₅F₇O₃Si₃

Guidance literature:: Multi-step reaction with 10 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.25 h / 5 - 20 °C

2.1: sodium acetate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.5 - 1.5 h / 5 - 20 °C

3.1: pyridine / 1 - 2 h / 20 °C

4.1: selenium(IV) oxide; di-tert-butyl peroxide / 1,4-dioxane; nonane / 22 - 37 h / 85 °C

5.1: diethylamino-sulfur trifluoride / Trichloroethylene / 0.33 h / -75 °C

6.1: triphenylphosphine / tris(3,5-dimethylpyrazolyl)hydriborate rhenium trioxide / toluene / 20 h / 100 °C

7.1: sodium methylate / methanol / 1 h / 20 °C

8.1: bis(trichloromethyl) carbonate / hexane / 0.5 h / 0 °C

8.2: 1 h / 0 - 20 °C

9.1: sodium hydride / N,N-dimethyl-formamide / 0.75 h / 10 - 20 °C

9.2: 3 h / -60 - 20 °C

10.1: n-butyllithium / 0.33 h / -70 °C

10.2: 4.5 h

With selenium(IV) oxide; n-butyllithium; di-tert-butyl peroxide; bis(trichloromethyl) carbonate; diethylamino-sulfur trifluoride; tetrabutyl ammonium fluoride; sodium methylate; sodium acetate; sodium hydride; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; tris(3,5-dimethylpyrazolyl)hydriborate rhenium trioxide; In tetrahydrofuran; 1,4-dioxane; pyridine; methanol; nonane; hexane; dichloromethane; Trichloroethylene; N,N-dimethyl-formamide; toluene;