bis((α,αdimethylbenzyl)oxy)bis(2,2,6,6-tetramethyl-3,5-heptanedionato)titanium(IV)

Base Information

• Chemical Name: bis((α,αdimethylbenzyl)oxy)bis(2,2,6,6-tetramethyl-3,5-heptanedionato)titanium(IV)
• CAS No.: 84848-15-7
• Molecular Formula: C₄₀H₆₀O₆Ti
• Molecular Weight: 684.793
• Mol file: 84848-15-7.mol

Synonyms:bis((α,αdimethylbenzyl)oxy)bis(2,2,6,6-tetramethyl-3,5-heptanedionato)titanium(IV)

Chemical Property of bis((α,αdimethylbenzyl)oxy)bis(2,2,6,6-tetramethyl-3,5-heptanedionato)titanium(IV)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of bis((α,αdimethylbenzyl)oxy)bis(2,2,6,6-tetramethyl-3,5-heptanedionato)titanium(IV)

There total 1 articles about bis((α,αdimethylbenzyl)oxy)bis(2,2,6,6-tetramethyl-3,5-heptanedionato)titanium(IV) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2,2,6,6-tetramethylheptane-3,5-dione (1118-71-4) + Ti(OC(C6H5)(CH3)2)4 → bis((α,αdimethylbenzyl)oxy)bis(2,2,6,6-tetramethyl-3,5-heptanedionato)titanium(IV) (84848-15-7)

Guidance literature:

In dichloromethane; byproducts: α,α-dimethylbenzyl alcohol; heated at 155°C for 2 h under N2, then heated in vacuo at 110°C for several days; kept for several weeks in vacuo; elem. anal.;

DOI:10.1021/ja00346a004

upstream raw materials:

2,2,6,6-tetramethylheptane-3,5-dione

Refernces