(S,S,RS)-<1-(cyclohexylmethyl)-4-oxo-2-<(tetrahydro-2H-pyran-2-yl)oxy>hexyl>carbamic acid 1,1-dimethylethyl ester

Base Information

• Chemical Name: (S,S,RS)-<1-(cyclohexylmethyl)-4-oxo-2-<(tetrahydro-2H-pyran-2-yl)oxy>hexyl>carbamic acid 1,1-dimethylethyl ester
• CAS No.: 131099-28-0
• Molecular Formula: C₂₃H₄₁NO₅
• Molecular Weight: 411.582

Synonyms:(S,S,RS)-<1-(cyclohexylmethyl)-4-oxo-2-<(tetrahydro-2H-pyran-2-yl)oxy>hexyl>carbamic acid 1,1-dimethylethyl ester

Chemical Property of (S,S,RS)-<1-(cyclohexylmethyl)-4-oxo-2-<(tetrahydro-2H-pyran-2-yl)oxy>hexyl>carbamic acid 1,1-dimethylethyl ester

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Technology Process of (S,S,RS)-<1-(cyclohexylmethyl)-4-oxo-2-<(tetrahydro-2H-pyran-2-yl)oxy>hexyl>carbamic acid 1,1-dimethylethyl ester

There total 2 articles about (S,S,RS)-<1-(cyclohexylmethyl)-4-oxo-2-<(tetrahydro-2H-pyran-2-yl)oxy>hexyl>carbamic acid 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

ethylmagnesium bromide (925-90-6) + (2S,3S)-2-Cyclohexylmethyl-5-oxo-3-(tetrahydro-pyran-2-yloxy)-pyrrolidine-1-carboxylic acid tert-butyl ester (131232-45-6) → (S,S,RS)-<1-(cyclohexylmethyl)-4-oxo-2-<(tetrahydro-2H-pyran-2-yl)oxy>hexyl>carbamic acid 1,1-dimethylethyl ester (131099-28-0)

Guidance literature:

In tetrahydrofuran; for 0.5h;

DOI:10.1021/jm00092a006

Reference yield: 57.0%

ethylmagnesium bromide (925-90-6) + (2S,3S)-2-Cyclohexylmethyl-5-oxo-3-(tetrahydro-pyran-2-yloxy)-pyrrolidine-1-carboxylic acid tert-butyl ester (131232-45-6) → (S,S,RS)-<1-(cyclohexylmethyl)-4-oxo-2-<(tetrahydro-2H-pyran-2-yl)oxy>hexyl>carbamic acid 1,1-dimethylethyl ester (131099-28-0) + 2-Cyclohexylmethyl-5-ethyl-pyrrole-1-carboxylic acid tert-butyl ester

Guidance literature:

In tetrahydrofuran; at 10 ℃; for 0.5h;

DOI:10.1080/00397919308013294

Reference yield: 93.0%

(S,S,RS)-<1-(cyclohexylmethyl)-4-oxo-2-<(tetrahydro-2H-pyran-2-yl)oxy>hexyl>carbamic acid 1,1-dimethylethyl ester (131099-28-0) → (S,S,RS,RS)-<1-(cylohexylmethyl)-4-hydroxy-2-<(tetrahydro-2H-pyran-2-yl)oxy>hexyl>carbamic acid 1,1-dimethylester (131099-29-1,131176-51-7)

Guidance literature:

With potassium borohydride; In methanol; water; for 2h; Ambient temperature;

DOI:10.1080/00397919308013294

upstream raw materials:

ethylmagnesium bromide

(2S,3S)-2-Cyclohexylmethyl-5-oxo-3-(tetrahydro-pyran-2-yloxy)-pyrrolidine-1-carboxylic acid tert-butyl ester

Downstream raw materials:

(S,S,RS,RS)-<1-(cylohexylmethyl)-4-hydroxy-2-<(tetrahydro-2H-pyran-2-yl)oxy>hexyl>carbamic acid 1,1-dimethylester

<2S-(2R*,3R*,5S*)>-2-amino-1-cyclohexyl-3,5-heptanediol hydrochloride

<2S-(2R*,3R*,5S*)>-2-amino-1-cyclohexyl-3,5-heptanediol

5(S)-2-amino-1-cyclohexyl-3,5-dihydroxyheptane

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