C₂₃H₂₄ClNO₅

Base Information

Chemical Name:C₂₃H₂₄ClNO₅
CAS No.:1234064-64-2
Molecular Formula:C₂₃H₂₄ClNO₅
Molecular Weight:429.9
Hs Code.:

C<sub>23</sub>H<sub>24</sub>ClNO<sub>5</sub>

Synonyms:C₂₃H₂₄ClNO₅

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Chemical Property of C₂₃H₂₄ClNO₅

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Technology Process of C₂₃H₂₄ClNO₅

There total 4 articles about C₂₃H₂₄ClNO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 1234064-61-9
C₂₃H₂₆ClNO₆

: 1234064-64-2
C₂₃H₂₄ClNO₅

Guidance literature:: With 2,5,8,9-tetraaza-1-phosphabicyclo[3.3.3]undecane 2,8,9-tris(1-methylethyl); In benzene; at 40 - 50 ℃; Molecular sieve;
DOI:10.1021/ja101740k

Reference yield:

: 131088-02-3
2,4-dihydroxy-5-chlorobenzaldehyde

: 1234064-64-2
C₂₃H₂₄ClNO₅

Guidance literature:: Multi-step reaction with 3 steps

1: sodium iodide; sodium hydrogencarbonate / acetonitrile / 16 h / 80 °C / Inert atmosphere

2: diisopropyl-carbodiimide / dmap / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

3: 2,5,8,9-tetraaza-1-phosphabicyclo[3.3.3]undecane 2,8,9-tris(1-methylethyl) / benzene / 17 h / 40 - 50 °C / Molecular sieve; Inert atmosphere

With sodium hydrogencarbonate; sodium iodide; 2,5,8,9-tetraaza-1-phosphabicyclo[3.3.3]undecane 2,8,9-tris(1-methylethyl); diisopropyl-carbodiimide; dmap; In dichloromethane; acetonitrile; benzene;

Reference yield:

: 1043920-04-2
4-(benzyloxy)-5-chloro-2-hydroxybenzaldehyde

: 1234064-64-2
C₂₃H₂₄ClNO₅

Guidance literature:: Multi-step reaction with 2 steps

1: diisopropyl-carbodiimide / dmap / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

2: 2,5,8,9-tetraaza-1-phosphabicyclo[3.3.3]undecane 2,8,9-tris(1-methylethyl) / benzene / 17 h / 40 - 50 °C / Molecular sieve; Inert atmosphere

With 2,5,8,9-tetraaza-1-phosphabicyclo[3.3.3]undecane 2,8,9-tris(1-methylethyl); diisopropyl-carbodiimide; dmap; In dichloromethane; benzene;