ethyl 10-iodo-3-oxo-2-(triphenylphosphoranylidene)-4-(E),9(Z)-decadienoate

Base Information

Chemical Name:ethyl 10-iodo-3-oxo-2-(triphenylphosphoranylidene)-4-(E),9(Z)-decadienoate
CAS No.:107408-28-6
Molecular Formula:C₃₀H₃₀IO₃P
Molecular Weight:596.445
Hs Code.:

Synonyms:ethyl 10-iodo-3-oxo-2-(triphenylphosphoranylidene)-4-(E),9(Z)-decadienoate

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Chemical Property of ethyl 10-iodo-3-oxo-2-(triphenylphosphoranylidene)-4-(E),9(Z)-decadienoate

Chemical Property:

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Technology Process of ethyl 10-iodo-3-oxo-2-(triphenylphosphoranylidene)-4-(E),9(Z)-decadienoate

There total 3 articles about ethyl 10-iodo-3-oxo-2-(triphenylphosphoranylidene)-4-(E),9(Z)-decadienoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 78980-76-4
diethyl <2,4-dioxo-4-ethoxy-3-(triphenylphosphoranylidene)butyl>-phosphonate

: 107408-27-5
(Z)-6-iodohex-5-enal

: 107408-28-6
ethyl 10-iodo-3-oxo-2-(triphenylphosphoranylidene)-4-(E),9(Z)-decadienoate

Guidance literature:: With sodium hydride; isopropyl alcohol; In tetrahydrofuran;

Reference yield:

: 132716-07-5,106335-91-5
(Z)-6-iodo-5-hexene-1-ol

: 107408-28-6
ethyl 10-iodo-3-oxo-2-(triphenylphosphoranylidene)-4-(E),9(Z)-decadienoate

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / pyridinium chlorochromate / CH₂Cl₂ / 1 h

2: 78 percent / NaH, 2-propanol / tetrahydrofuran

With sodium hydride; isopropyl alcohol; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane;

Reference yield:

: 107408-26-4
2-((Z)-6-Iodo-hex-5-enyloxy)-tetrahydro-pyran

: 107408-28-6
ethyl 10-iodo-3-oxo-2-(triphenylphosphoranylidene)-4-(E),9(Z)-decadienoate

Guidance literature:: Multi-step reaction with 3 steps

1: 60percent aq. HOAc / 3 h

2: 71 percent / pyridinium chlorochromate / CH₂Cl₂ / 1 h

3: 78 percent / NaH, 2-propanol / tetrahydrofuran

With sodium hydride; acetic acid; isopropyl alcohol; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane;