17-Benzyl-7,9,20-trimethyl-3,13,17-triaza-tricyclo[13.3.1.1^6,10]icosa-1⁽¹⁸⁾,6,8,10⁽²⁰⁾,15-pentaene-2,14-dione

Base Information

• Chemical Name: 17-Benzyl-7,9,20-trimethyl-3,13,17-triaza-tricyclo[13.3.1.1^6,10]icosa-1⁽¹⁸⁾,6,8,10⁽²⁰⁾,15-pentaene-2,14-dione
• CAS No.: 75340-06-6
• Molecular Formula: C₂₇H₃₁N₃O₂
• Molecular Weight: 429.562

Synonyms:17-Benzyl-7,9,20-trimethyl-3,13,17-triaza-tricyclo[13.3.1.1^6,10]icosa-1⁽¹⁸⁾,6,8,10⁽²⁰⁾,15-pentaene-2,14-dione

Chemical Property of 17-Benzyl-7,9,20-trimethyl-3,13,17-triaza-tricyclo[13.3.1.1^6,10]icosa-1⁽¹⁸⁾,6,8,10⁽²⁰⁾,15-pentaene-2,14-dione

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 17-Benzyl-7,9,20-trimethyl-3,13,17-triaza-tricyclo[13.3.1.1^6,10]icosa-1⁽¹⁸⁾,6,8,10⁽²⁰⁾,15-pentaene-2,14-dione

There total 4 articles about 17-Benzyl-7,9,20-trimethyl-3,13,17-triaza-tricyclo[13.3.1.1^6,10]icosa-1⁽¹⁸⁾,6,8,10⁽²⁰⁾,15-pentaene-2,14-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

17-Benzyl-7,9,20-trimethyl-2,14-dioxo-3,13-diaza-17-azonia-tricyclo[13.3.1.16,10]icosa-1(18),6,8,10(20),15(19),16-hexaene; bromide (75340-04-4) → 17-Benzyl-7,9,20-trimethyl-3,13,17-triaza-tricyclo[13.3.1.16,10]icosa-1(18),6,8,10(20),15-pentaene-2,14-dione (75340-06-6)

Guidance literature:

With 1-Benzyl-1,4-dihydronicotinamide; In methanol; at 50 ℃; for 3h; dark;

DOI:10.1021/ja00325a020

Reference yield:

3,5-Pyridinedicarboxylic acid (499-81-0) → 17-Benzyl-7,9,20-trimethyl-3,13,17-triaza-tricyclo[13.3.1.16,10]icosa-1(18),6,8,10(20),15-pentaene-2,14-dione (75340-06-6)

Guidance literature:

Multi-step reaction with 4 steps

1: 85 percent / tionyl chloride / Heating

2: 10 percent / triethylamine / toluene / 50 h / Ambient temperature

3: 70 percent / 1 h / 80 °C

4: β-NADH / H2O / 20 °C / pH=7

With thionyl chloride; 1,4-dihydronicotinamide adenine dinucleotide; triethylamine; In water; toluene;

DOI:10.1021/ja00325a020

Reference yield:

pyridine-3,5-dicarbonyl dichloride (15074-61-0) → 17-Benzyl-7,9,20-trimethyl-3,13,17-triaza-tricyclo[13.3.1.16,10]icosa-1(18),6,8,10(20),15-pentaene-2,14-dione (75340-06-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 10 percent / triethylamine / toluene / 50 h / Ambient temperature

2: 70 percent / 1 h / 80 °C

3: β-NADH / H2O / 20 °C / pH=7

With 1,4-dihydronicotinamide adenine dinucleotide; triethylamine; In water; toluene;

DOI:10.1021/ja00325a020

upstream raw materials:

17-Benzyl-7,9,20-trimethyl-2,14-dioxo-3,13-diaza-17-azonia-tricyclo[13.3.1.1^6,10]icosa-1⁽¹⁸⁾,6,8,10⁽²⁰⁾,15⁽¹⁹⁾,16-hexaene; bromide

3,5-Pyridinedicarboxylic acid

pyridine-3,5-dicarbonyl dichloride

7,9,20-Trimethyl-3,13,17-triaza-tricyclo[13.3.1.1^6,10]icosa-1⁽¹⁸⁾,6,8,10⁽²⁰⁾,15⁽¹⁹⁾,16-hexaene-2,14-dione

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 75340-06-6 17-Benzyl-7,9,20-trimethyl-3,13,17-triaza-tricyclo[13.3.1.1^6,10]icosa-1⁽¹⁸⁾,6,8,10⁽²⁰⁾,15-pentaene-2,14-dione

Send

Send

Metric Ton KG G Pound L ML

Send

Send