thallium(I) bis-3,5-trifluoromethylphenoxide

Base Information

Chemical Name:thallium(I) bis-3,5-trifluoromethylphenoxide
CAS No.:811433-47-3
Molecular Formula:C₈H₃F₆O*Tl
Molecular Weight:433.485
Hs Code.:

Synonyms:thallium(I) bis-3,5-trifluoromethylphenoxide

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Chemical Property of thallium(I) bis-3,5-trifluoromethylphenoxide

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Technology Process of thallium(I) bis-3,5-trifluoromethylphenoxide

There total 1 articles about thallium(I) bis-3,5-trifluoromethylphenoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.4%

: 349-58-6
3,5-bis-(trifluoromethyl)phenol

: 20398-06-5
thallium (I) ethoxide

: 811433-47-3
thallium(I) bis-3,5-trifluoromethylphenoxide

Guidance literature:: In toluene; at room temp. on a Schlenk line or under N2 or Ar; TlOC2H5 added to HOC6H3(CF3)2 in toluene, stirred overnight; evapd. (vac.), dissolved in warm toluene, filtered, cooled, layered withroom-temp. hexanes;
DOI:10.1021/ic0493954

Reference yield: 90.0%

: 14264-16-5,53996-95-5,62075-39-2,39716-73-9
bis(triphenylphosphine)nickel(II) chloride

: 811433-47-3
thallium(I) bis-3,5-trifluoromethylphenoxide

: 866886-04-6
[((C₆H₅)3P)2Ni(OC₆H₃(CF₃)2)2]

Guidance literature:: In dichloromethane; byproducts: TlCl; all manipulations under N2 or Ar atm.; Tl compd. dissolved in CH2Cl2, Nicompd. added, stirred overnight at room temp.; filtered, concd. in vac., recrystd. from CH2Cl2/hexane (1:1); elem. anal.;
DOI:10.1016/j.poly.2005.06.012

Reference yield: 52.0%

: 811433-47-3
thallium(I) bis-3,5-trifluoromethylphenoxide

: 108-88-3,15644-74-3,16713-13-6
toluene

: cobalt(II) iodide

: [Tl₂Co(bis-3,5-trifluoromethylphenoxide)4] * 2(toluene)

Guidance literature:: In tetrahydrofuran; byproducts: TlI; at room temp. on a Schlenk line or under N2 or Ar; CoI2 added to a soln.of Tl compd., stirred; filtered (Celite), evapd. (vac.), triturated with hexane, dissolved in toluene, filtered, layered with hexane, stored at -30°C; elem. anal.;
DOI:10.1021/ic0493954