Technology Process of C25H29N5O3
There total 5 articles about C25H29N5O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
at 55 ℃;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C
2: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 5 h / 0 - 20 °C
3: copper(l) iodide; potassium carbonate / dimethyl sulfoxide / 100 °C
4: sodium hydroxide / tetrahydrofuran; ethanol / 4 h / 70 °C
5: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 55 °C
With
copper(l) iodide; thionyl chloride; 1-hydroxy-7-aza-benzotriazole; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide;
In
tetrahydrofuran; ethanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 5 h / 0 - 20 °C
2: copper(l) iodide; potassium carbonate / dimethyl sulfoxide / 100 °C
3: sodium hydroxide / tetrahydrofuran; ethanol / 4 h / 70 °C
4: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 55 °C
With
copper(l) iodide; thionyl chloride; 1-hydroxy-7-aza-benzotriazole; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; sodium hydroxide;
In
tetrahydrofuran; ethanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;