C₁₂H₁₄FIO₂

Base Information

Chemical Name:C₁₂H₁₄FIO₂
CAS No.:1402585-14-1
Molecular Formula:C₁₂H₁₄FIO₂
Molecular Weight:336.145
Hs Code.:

C<sub>12</sub>H<sub>14</sub>FIO<sub>2</sub>

Synonyms:C₁₂H₁₄FIO₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₂H₁₄FIO₂

Chemical Property:

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Technology Process of C₁₂H₁₄FIO₂

There total 4 articles about C₁₂H₁₄FIO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 1402585-13-0
C₁₂H₁₆FNO₂

: 1402585-14-1
C₁₂H₁₄FIO₂

Guidance literature:: With toluene-4-sulfonic acid; potassium iodide; sodium nitrite; In water; acetonitrile; at 10 - 20 ℃;

Reference yield:

: 1402585-12-9
C₁₂H₁₄FNO₄

: 1402585-14-1
C₁₂H₁₄FIO₂

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen; palladium 10% on activated carbon / methanol / 2 h

2: sodium nitrite; toluene-4-sulfonic acid; potassium iodide / water; acetonitrile / 10 - 20 °C

With palladium 10% on activated carbon; hydrogen; toluene-4-sulfonic acid; potassium iodide; sodium nitrite; In methanol; water; acetonitrile;

Reference yield:

: 107-59-5
tert-Butyl chloroacetate

: 1402585-14-1
C₁₂H₁₄FIO₂

Guidance literature:: Multi-step reaction with 3 steps

1: potassium tert-butylate / 1-methyl-pyrrolidin-2-one / 0.5 h / -20 - -10 °C / Inert atmosphere

2: hydrogen; palladium 10% on activated carbon / methanol / 2 h

3: sodium nitrite; toluene-4-sulfonic acid; potassium iodide / water; acetonitrile / 10 - 20 °C

With palladium 10% on activated carbon; potassium tert-butylate; hydrogen; toluene-4-sulfonic acid; potassium iodide; sodium nitrite; In 1-methyl-pyrrolidin-2-one; methanol; water; acetonitrile;