Technology Process of C27H27N3O3S
There total 9 articles about C27H27N3O3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
N,N-dimethyl-formamide;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / 1-methyl-pyrrolidin-2-one / 80 °C
2: hydrogen / palladium on activated carbon / methanol / 40 °C
3: 1,4-dioxane / 3 h / Reflux
4: N,N-dimethyl-formamide / 20 °C
With
hydrogen; potassium carbonate;
palladium on activated carbon;
In
1,4-dioxane; 1-methyl-pyrrolidin-2-one; methanol; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: dmap / dichloromethane / Reflux
2: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 100 °C
3: caesium carbonate / water; dimethyl sulfoxide / 110 °C / Inert atmosphere
4: hydrogenchloride; water / 3 h / Reflux
5: N,N-dimethyl-formamide / 20 °C
With
hydrogenchloride; dmap; water; potassium acetate; caesium carbonate;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride;
In
dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;