(-)-(2S,3S)-N-benzoyl-4-hydroxy-2,3-bis(methoxymethoxy)butylamine

Base Information

Chemical Name:(-)-(2S,3S)-N-benzoyl-4-hydroxy-2,3-bis(methoxymethoxy)butylamine
CAS No.:114486-19-0
Molecular Formula:C₁₅H₂₃NO₆
Molecular Weight:313.351
Hs Code.:

Synonyms:(-)-(2S,3S)-N-benzoyl-4-hydroxy-2,3-bis(methoxymethoxy)butylamine

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Chemical Property of (-)-(2S,3S)-N-benzoyl-4-hydroxy-2,3-bis(methoxymethoxy)butylamine

Chemical Property:

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Technology Process of (-)-(2S,3S)-N-benzoyl-4-hydroxy-2,3-bis(methoxymethoxy)butylamine

There total 6 articles about (-)-(2S,3S)-N-benzoyl-4-hydroxy-2,3-bis(methoxymethoxy)butylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 114486-17-8
(-)-(2S,3S)-N-benzoyl-4-benzyloxy-2,3-dimethoxymethoxybutylamine

: 114486-19-0
(-)-(2S,3S)-N-benzoyl-4-hydroxy-2,3-bis(methoxymethoxy)butylamine

Guidance literature:: With hydrogen; palladium on activated charcoal; for 84h; under 760 Torr;

Reference yield:

: 136918-14-4,85-41-6
phthalimide

: 114486-19-0
(-)-(2S,3S)-N-benzoyl-4-hydroxy-2,3-bis(methoxymethoxy)butylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / triphenylphosphine/diethyl azodicarboxylate / tetrahydrofuran / 0.17 h / Ambient temperature

2: 1.) hydrazine hydrate, 2.) triethylamine / 1.) ethanol, reflux, 2.5 h; 2.) methylene dichloride, room temp., 17 h

3: 100 percent / H₂ / 10percent palladium-carbon / 84 h / 760 Torr

With hydrogen; hydrazine hydrate; triethylamine; triphenylphosphine; diethylazodicarboxylate; palladium on activated charcoal; In tetrahydrofuran;

Reference yield:

: 99891-36-8
(-)-(2S,3S)-2,3-bis(methoxymethoxy)butane-1,4-diol

: 114486-19-0
(-)-(2S,3S)-N-benzoyl-4-hydroxy-2,3-bis(methoxymethoxy)butylamine

Guidance literature:: Multi-step reaction with 4 steps

1: 79 percent / sodium hydride / dimethylformamide / 1.) -40 to - 20 deg C, 0.5 h; 2.) -20 to room temp., 10 h

2: 92 percent / triphenylphosphine/diethyl azodicarboxylate / tetrahydrofuran / 0.17 h / Ambient temperature

3: 1.) hydrazine hydrate, 2.) triethylamine / 1.) ethanol, reflux, 2.5 h; 2.) methylene dichloride, room temp., 17 h

4: 100 percent / H₂ / 10percent palladium-carbon / 84 h / 760 Torr

With hydrogen; sodium hydride; hydrazine hydrate; triethylamine; triphenylphosphine; diethylazodicarboxylate; palladium on activated charcoal; In tetrahydrofuran; N,N-dimethyl-formamide;